Silane, trimethyl[3-methyl-1-(phenylthio)-2-butenyl]-

Base Information

Chemical Name:Silane, trimethyl[3-methyl-1-(phenylthio)-2-butenyl]-
CAS No.:88410-22-4
Molecular Formula:C14H22SSi
Molecular Weight:250.48
Hs Code.:
DSSTox Substance ID:DTXSID20460960
Nikkaji Number:J2.112.346C

Synonyms:Silane, trimethyl[3-methyl-1-(phenylthio)-2-butenyl]-;88410-22-4;DTXSID20460960

Suppliers and Price of Silane, trimethyl[3-methyl-1-(phenylthio)-2-butenyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Silane, trimethyl[3-methyl-1-(phenylthio)-2-butenyl]-

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:4
Exact Mass:250.12114841
Heavy Atom Count:16
Complexity:230

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(=CC([Si](C)(C)C)SC1=CC=CC=C1)C

Technology Process of Silane, trimethyl[3-methyl-1-(phenylthio)-2-butenyl]-

There total 6 articles about Silane, trimethyl[3-methyl-1-(phenylthio)-2-butenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 88410-17-7
(1-Benzenesulfinyl-3-methyl-buta-1,2-dienyl)-trimethyl-silane

: 88410-22-4
trimethyl[3-methyl-1-(phenylthio)but-2-enyl]silane

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; at -50 ℃;
DOI:10.1016/S0040-4039(00)85927-4

Reference yield: 21.0%

: 75-77-4
chloro-trimethyl-silane

: 117785-43-0
(4-methyl-1-phenylpent-3-en-2-yl)(phenyl)sulfane

: 88410-22-4
trimethyl[3-methyl-1-(phenylthio)but-2-enyl]silane

Guidance literature:: (4-methyl-1-phenylpent-3-en-2-yl)(phenyl)sulfane; With lithium 4,4′-di-tert-butylbiphenylide; In tetrahydrofuran; at -11 ℃;

chloro-trimethyl-silane; In tetrahydrofuran; at -11 ℃;
DOI:10.1021/jo049237u

Reference yield:

: 5272-33-3
2-methyl-4-(trimethylsilyl)but-3-yn-2-ol

: 88410-22-4
trimethyl[3-methyl-1-(phenylthio)but-2-enyl]silane

Guidance literature:: Multi-step reaction with 2 steps

1: 56 percent / Et₃N / diethyl ether / -20 °C

2: 65 percent / LiAlH₄ / diethyl ether / -50 °C

With lithium aluminium tetrahydride; triethylamine; In diethyl ether;
DOI:10.1016/S0040-4039(00)85927-4