N-[3-(Methylamino)-4-nitrophenyl]methanesulfonamide

Base Information

Chemical Name:N-[3-(Methylamino)-4-nitrophenyl]methanesulfonamide
CAS No.:88413-07-4
Molecular Formula:C8H11N3O4S
Molecular Weight:245.259
Hs Code.:
DSSTox Substance ID:DTXSID90546109
Wikidata:Q82423819

Synonyms:88413-07-4;N-[3-(Methylamino)-4-nitrophenyl]methanesulfonamide;DTXSID90546109

Suppliers and Price of N-[3-(Methylamino)-4-nitrophenyl]methanesulfonamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of N-[3-(Methylamino)-4-nitrophenyl]methanesulfonamide

Chemical Property:

XLogP3:1.3
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:3
Exact Mass:245.04702701
Heavy Atom Count:16
Complexity:345

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CNC1=C(C=CC(=C1)NS(=O)(=O)C)[N+](=O)[O-]

Technology Process of N-[3-(Methylamino)-4-nitrophenyl]methanesulfonamide

There total 9 articles about N-[3-(Methylamino)-4-nitrophenyl]methanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 712-33-4
3-chloro-4-nitroacetanilide

: 88413-07-4
3-(methamine)-4-nitro-N-(methylsulfonyl)benzenamine

Guidance literature:: Multi-step reaction with 4 steps

1: 5 h / 100 °C

2: aq. KOH / ethanol

3: pyridine / 3 h / 0 - 20 °C

4: aq. HCl / ethanol / 1 h / Heating

With pyridine; hydrogenchloride; potassium hydroxide; In ethanol;
DOI:10.1021/jm00159a035

Reference yield:

: 88413-26-7
3-(methylamino)-4-nitroacetanilide

: 88413-07-4
3-(methamine)-4-nitro-N-(methylsulfonyl)benzenamine

Guidance literature:: Multi-step reaction with 2 steps

1: 2 N HCl / ethanol / 1 h / Heating

2: pyridine / 1.) 20 deg C, 1 h, 2.) 100 deg C, 15 min

With pyridine; hydrogenchloride; In ethanol;
DOI:10.1021/jm00369a022