{[1-(1-Methoxycyclohexyl)-2-methylidenecyclobutyl]oxy}(trimethyl)silane

Base Information

Chemical Name:{[1-(1-Methoxycyclohexyl)-2-methylidenecyclobutyl]oxy}(trimethyl)silane
CAS No.:88441-52-5
Molecular Formula:C15H28O2Si
Molecular Weight:268.472
Hs Code.:
DSSTox Substance ID:DTXSID20531280

Synonyms:88441-52-5;DTXSID20531280;{[1-(1-Methoxycyclohexyl)-2-methylidenecyclobutyl]oxy}(trimethyl)silane

Suppliers and Price of {[1-(1-Methoxycyclohexyl)-2-methylidenecyclobutyl]oxy}(trimethyl)silane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of {[1-(1-Methoxycyclohexyl)-2-methylidenecyclobutyl]oxy}(trimethyl)silane

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:268.185856666
Heavy Atom Count:18
Complexity:326

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1(CCCCC1)C2(CCC2=C)O[Si](C)(C)C

Technology Process of {[1-(1-Methoxycyclohexyl)-2-methylidenecyclobutyl]oxy}(trimethyl)silane

There total 3 articles about {[1-(1-Methoxycyclohexyl)-2-methylidenecyclobutyl]oxy}(trimethyl)silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1779-49-3
Methyltriphenylphosphonium bromide

: 69152-08-5
2-(1-methoxycyclohexyl)-2-(trimethylsiloxy)cyclobutanone

: 88441-52-5
1-(1-methoxycyclohexyl)-2-methylene-1-(trimethylsiloxy)cyclobutane

Guidance literature:: With potassium hydride; In tetrahydrofuran; at 20 ℃; for 3h;
DOI:10.1021/ja00318a035

Reference yield:

: 17082-61-0
1,2-bis(trimethylsiloxy)cyclobutene

: 88441-52-5
1-(1-methoxycyclohexyl)-2-methylene-1-(trimethylsiloxy)cyclobutane

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / BF₃*Et₂O / CH₂Cl₂ / 0.2 h

2: 83 percent / potassium hydride / tetrahydrofuran / 3 h / 20 °C

With boron trifluoride diethyl etherate; potassium hydride; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja00318a035

Reference yield:

: 933-40-4
cycloxexanone dimethyl ketal

: 88441-52-5
1-(1-methoxycyclohexyl)-2-methylene-1-(trimethylsiloxy)cyclobutane

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / BF₃*Et₂O / CH₂Cl₂ / 0.2 h

2: 83 percent / potassium hydride / tetrahydrofuran / 3 h / 20 °C

With boron trifluoride diethyl etherate; potassium hydride; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja00318a035