2,5-dichloro-N,N-dimethylbenzenesulfonamide

Base Information

Chemical Name:2,5-dichloro-N,N-dimethylbenzenesulfonamide
CAS No.:88522-19-4
Molecular Formula:C8H9Cl2NO2S
Molecular Weight:254.137
Hs Code.:
DSSTox Substance ID:DTXSID80354694
Wikidata:Q82133015
ChEMBL ID:CHEMBL3956863

Synonyms:2,5-dichloro-N,N-dimethylbenzenesulfonamide;88522-19-4;2,5-dichloro-N,N-dimethylbenzene-1-sulfonamide;CHEMBL3956863;DTXSID80354694;STK066754;AKOS000384241;CS-0322113;AG-690/11633966;Z45527558

Suppliers and Price of 2,5-dichloro-N,N-dimethylbenzenesulfonamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 2,5-dichloro-N,N-dimethylbenzenesulfonamide

Chemical Property:

XLogP3:2.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:252.9731051
Heavy Atom Count:14
Complexity:286

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN(C)S(=O)(=O)C1=C(C=CC(=C1)Cl)Cl

Technology Process of 2,5-dichloro-N,N-dimethylbenzenesulfonamide

There total 3 articles about 2,5-dichloro-N,N-dimethylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 103-83-3
N,N'-dimethylbenzylamine

: 5402-73-3
2,5-dichlorobenzenesulphonyl chloride

: 88522-19-4
N,N-dimethyl-2,5-dichlorobenzenesulfonamide

Guidance literature:: With sodium sulfate; In water; at 20 ℃; for 3.2h; Electrochemical reaction;
DOI:10.1039/c7gc03141f

Reference yield: 76.0%

: 103-83-3
N,N'-dimethylbenzylamine

: 6775-66-2
2,5-dichlorobenzenesulfonylhydrazide

: 88522-19-4
N,N-dimethyl-2,5-dichlorobenzenesulfonamide

Guidance literature:: With sodium sulfate; In water; acetonitrile; at 20 ℃; for 9h; Electrochemical reaction;
DOI:10.1039/c7gc03141f

Reference yield:

: 5402-73-3
2,5-dichlorobenzenesulphonyl chloride

: 88522-19-4
N,N-dimethyl-2,5-dichlorobenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / tetrahydrofuran / 0.25 h / 10 °C

2: sodium sulfate / water; acetonitrile / 9 h / 20 °C / Electrochemical reaction

With hydrazine hydrate; sodium sulfate; In tetrahydrofuran; water; acetonitrile;
DOI:10.1039/c7gc03141f