2-Bromo-N-(2-cyanophenyl)butanamide

Base Information

Chemical Name:2-Bromo-N-(2-cyanophenyl)butanamide
CAS No.:88629-04-3
Molecular Formula:C11H11BrN2O
Molecular Weight:267.125
Hs Code.:
DSSTox Substance ID:DTXSID50518988

Synonyms:2-Bromo-N-(2-cyanophenyl)butanamide;88629-04-3;DTXSID50518988;AKOS012152069

Suppliers and Price of 2-Bromo-N-(2-cyanophenyl)butanamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 2-Bromo-N-(2-cyanophenyl)butanamide

Chemical Property:

XLogP3:2.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:266.00548
Heavy Atom Count:15
Complexity:271

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCC(C(=O)NC1=CC=CC=C1C#N)Br

Technology Process of 2-Bromo-N-(2-cyanophenyl)butanamide

There total 1 articles about 2-Bromo-N-(2-cyanophenyl)butanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 26074-52-2
2-bromo-butyryl bromide

: 1885-29-6
anthranilic acid nitrile

: 88629-04-3
N-(α-bromobutyryl)-2-cyanoanilide

Guidance literature:: With potassium carbonate; In dichloromethane; at 0 - 20 ℃;
DOI:10.1039/b819260j

Reference yield: 80.0%

: 88629-04-3
N-(α-bromobutyryl)-2-cyanoanilide

: 100-58-3
phenylmagnesium bromide

: 2,5-phenyl-2-ethyl-1,2,4,5-dihydro-[3H]-1,4-benzodiazepin-3-one

Guidance literature:: N-(α-bromobutyryl)-2-cyanoanilide; phenylmagnesium bromide; In tetrahydrofuran; Reflux;

With water; ammonium chloride; In tetrahydrofuran; for 1h;
DOI:10.1039/b819260j

Reference yield: 68.0%

: 88629-04-3
N-(α-bromobutyryl)-2-cyanoanilide

: 100-58-3
phenylmagnesium bromide

: 88629-06-5
2-ethyl-5-phenyl-4,5-dihydro-[3H]-1,4-benzodiazepin-3-one

Guidance literature:: N-(α-bromobutyryl)-2-cyanoanilide; phenylmagnesium bromide; In tetrahydrofuran; for 4h; Reflux;

With water; ammonium chloride; In tetrahydrofuran; for 1h;
DOI:10.1039/b819260j