Technology Process of 1-Propanol, 3-[[(4-methoxyphenyl)methylene]oxidoamino]-
There total 3 articles about 1-Propanol, 3-[[(4-methoxyphenyl)methylene]oxidoamino]- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: peroxyacetic acid / CH2Cl2 / 12 h / Ambient temperature
2: 1.) 10percent ethanolic H2SO4 2.) 20percent ethanolic KOH / 1.) room temperature, 24h 2.) room temperature, 24h
3: 1.) 20percent HCl 2.) 20percent ethanolic KOH / 1.) 1h, room temperature 2.) ethanol, room temperature
With
hydrogenchloride; peracetic acid; potassium hydroxide; sulfuric acid;
In
dichloromethane;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1.) 10percent ethanolic H2SO4 2.) 20percent ethanolic KOH / 1.) room temperature, 24h 2.) room temperature, 24h
2: 1.) 20percent HCl 2.) 20percent ethanolic KOH / 1.) 1h, room temperature 2.) ethanol, room temperature
With
hydrogenchloride; potassium hydroxide; sulfuric acid;
- Guidance literature:
-
With
hydrogenchloride; potassium hydroxide;
Yield given. Multistep reaction;
1.) 1h, room temperature 2.) ethanol, room temperature;