2-[(12-Fluorododec-3-YN-1-YL)oxy]oxane

Base Information

Chemical Name:2-[(12-Fluorododec-3-YN-1-YL)oxy]oxane
CAS No.:88730-57-8
Molecular Formula:C17H29FO2
Molecular Weight:
Hs Code.:
DSSTox Substance ID:DTXSID30538583

Synonyms:88730-57-8;2-[(12-FLUORODODEC-3-YN-1-YL)OXY]OXANE;SCHEMBL11064326;DTXSID30538583;ROVOAZBCHDNVBH-UHFFFAOYSA-N;12-fluoro-3-dodecyn-1-yl tetrahydropyranyl ether

Suppliers and Price of 2-[(12-Fluorododec-3-YN-1-YL)oxy]oxane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 2-[(12-Fluorododec-3-YN-1-YL)oxy]oxane

Chemical Property:

XLogP3:5.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:10
Exact Mass:284.21515833
Heavy Atom Count:20
Complexity:279

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CCOC(C1)OCCC#CCCCCCCCCF

Technology Process of 2-[(12-Fluorododec-3-YN-1-YL)oxy]oxane

There total 2 articles about 2-[(12-Fluorododec-3-YN-1-YL)oxy]oxane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 40365-61-5
2-(but-3-yn-1-yloxy)tetrahydropyran

: 593-12-4
1-bromo-8-fluorooctane

: 88730-57-8
1-<(2-Tetrahydropyranyl)oxy>-12-fluorododec-3-yne

Guidance literature:: With n-butyllithium; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; hexane; water; ethyl acetate;

Reference yield:

: 50816-19-8
8-bromooctanol

: 88730-57-8
1-<(2-Tetrahydropyranyl)oxy>-12-fluorododec-3-yne

Guidance literature:: Multi-step reaction with 2 steps

1: 61 percent / (diethylamino)sulfur trifluoride / CH₂Cl₂ / 1) -78 deg C, 2) 25 deg C

2: 1) n-butyllithium / 1) a) THF, -78 deg C, 1h, b) -5 deg C 5 min, 2) HMPA, room temperature

With n-butyllithium; diethylamino-sulfur trifluoride; In dichloromethane;
DOI:10.1021/jo00181a023