Benzamide, 2-amino-N,N-diethyl-4-methoxy-

Base Information

Chemical Name:Benzamide, 2-amino-N,N-diethyl-4-methoxy-
CAS No.:88733-50-0
Molecular Formula:C12H18N2O2
Molecular Weight:222.287
Hs Code.:
DSSTox Substance ID:DTXSID60467731
Wikidata:Q82294791

Synonyms:Benzamide, 2-amino-N,N-diethyl-4-methoxy-;88733-50-0;DTXSID60467731

Suppliers and Price of Benzamide, 2-amino-N,N-diethyl-4-methoxy-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Benzamide, 2-amino-N,N-diethyl-4-methoxy-

Chemical Property:

XLogP3:2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:222.136827821
Heavy Atom Count:16
Complexity:229

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCN(CC)C(=O)C1=C(C=C(C=C1)OC)N

Technology Process of Benzamide, 2-amino-N,N-diethyl-4-methoxy-

There total 3 articles about Benzamide, 2-amino-N,N-diethyl-4-methoxy- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 898534-16-2
4-ethynyl-2-isopropylaminothiazole

: 201230-82-2
carbon monoxide

: 109-89-7
diethylamine

: 153898-63-6
2-iodo-5-methoxyaniline

: 2-(2-isopropyloaminothiazol-4-yl)-7-methoxy-4a,8a-dihydro-1H-quinolin-4-one

: 88733-50-0
2-Amino-N,N-diethyl-4-methoxy-benzamide

Guidance literature:: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; at 120 ℃; for 6h; under 12928.7 Torr;
DOI:10.1021/jo060556q

Reference yield:

: 58755-70-7
1-iodo-4-methoxy-2-nitrobenzene

: 88733-50-0
2-Amino-N,N-diethyl-4-methoxy-benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / hydrazine monohydrate; graphite / ethanol / 8 h / Heating

2: PdCl₂(dppf) / 6 h / 120 °C / 12928.7 Torr

With pyrographite; hydrazine hydrate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In ethanol;
DOI:10.1021/jo060556q