Chromium,pentacarbonyl(pyridine)-, (OC-6-22)-

Base Information

Chemical Name:Chromium,pentacarbonyl(pyridine)-, (OC-6-22)-
CAS No.:14740-77-3
Molecular Formula:C10H5 Cr N O5
Molecular Weight:271.149
Hs Code.:
Mol file:14740-77-3.mol

Synonyms:(Pyridine)chromiumpentacarbonyl (6CI); Chromium, pentacarbonyl(pyridine)- (7CI,8CI);Pentacarbonyl(pyridine)chromium

Suppliers and Price of Chromium,pentacarbonyl(pyridine)-, (OC-6-22)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Chromium,pentacarbonyl(pyridine)-, (OC-6-22)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Chromium,pentacarbonyl(pyridine)-, (OC-6-22)-

There total 17 articles about Chromium,pentacarbonyl(pyridine)-, (OC-6-22)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.1%

: 1,4-bis(2-ethoxy-1,1,1,1,1-pentacarbonyl-1-chroma-1-ethen-2-yl)-2a-methyl-2,5-diphenyl-2a,3,6,7-tetrahydro-8-oxa-5a-azacyclobuta[d]indene

: 14740-77-3
pentacarbonyl(pyridine)chromium⁽⁰⁾

: 4-(2-ethoxy-1,1,1,1,1-pentacarbonyl-1-chroma-1-ethen-2-yl)-2a-methyl-2,5-diphenyl-2a,3,6,7-tetrahydro-8-oxa-5a-azacyclobuta[d]indene-1-carboxylic acid ethyl ester

Guidance literature:: With pyridine N-oxide; In dichloromethane; N2 atm.; complex was reacted with pyridine N-oxide in dry CH2Cl2 with stirring at ambient temp.; volatiles were removed under reduced pressure, chromy. on silica gel, hexane-CH2Cl2 1:1, volatiles were removed under reduced pressure, recrystd. from pentane at -20°C; elem. anal.;
DOI:10.1021/om049213d

Reference yield: 82.0%

: 110-86-1
pyridine

: 26160-57-6
pentacarbonyl(ethoxyphenylmethylene)chromium⁽⁰⁾

: 75-08-1
ethanethiol

: 14740-77-3
pentacarbonyl(pyridine)chromium⁽⁰⁾

: 70134-86-0
α-ethoxy-α-ethylthiotoluene

Guidance literature:: In tetrahydrofuran; under inert gas; Cr-complex and thio-compound in dry THF, heated (1 h, 70°C), addn. of pyridine (20°C), 24 h at 20°C; crystn.;