5-Bromo-6-(chloromethyl)benzo[d][1,3]dioxole

Base Information

Chemical Name:5-Bromo-6-(chloromethyl)benzo[d][1,3]dioxole
CAS No.:64603-67-4
Molecular Formula:C8H6 Br Cl O2
Molecular Weight:249.491
Hs Code.:2932999099
European Community (EC) Number:871-886-1
DSSTox Substance ID:DTXSID20368694
Wikidata:Q82155434

Synonyms:64603-67-4;5-Bromo-6-(chloromethyl)benzo[d][1,3]dioxole;5-bromo-6-(chloromethyl)-1,3-benzodioxole;5-bromo-6-(chloromethyl)-2H-1,3-benzodioxole;SCHEMBL11182069;DTXSID20368694;UOZXZWOFQWKKEZ-UHFFFAOYSA-N;MFCD06368742;AKOS015966223;6-bromo-3,4-methylenedioxybenzyl chloride;5-bromo-6-(chloromethyl)-1,3-dioxaindane;CS-0529270;FT-0760638;EN300-11529;5-Bromo-6-(chloromethyl);benzo[d][1,3]dioxole;Z57050099

Suppliers and Price of 5-Bromo-6-(chloromethyl)benzo[d][1,3]dioxole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
5-Bromo-6-(chloromethyl)benzo[d][1,3]dioxole 95+%
1g
$ 353.00

Chemenu
5-bromo-6-(chloromethyl)benzo[d][1,3]dioxole 95%
1g
$ 333.00

American Custom Chemicals Corporation
5-BROMO-6-(CHLOROMETHYL)-1,3-BENZODIOXOLE 95.00%
5G
$ 1928.08

American Custom Chemicals Corporation
5-BROMO-6-(CHLOROMETHYL)-1,3-BENZODIOXOLE 95.00%
2.5G
$ 1473.14

American Custom Chemicals Corporation
5-BROMO-6-(CHLOROMETHYL)-1,3-BENZODIOXOLE 95.00%
1G
$ 983.52

Alichem
5-Bromo-6-(chloromethyl)benzo[d][1,3]dioxole
1g
$ 400.00

AK Scientific
5-Bromo-6-(chloromethyl)benzo[d][1,3]dioxole
5g
$ 2378.00

AK Scientific
5-Bromo-6-(chloromethyl)benzo[d][1,3]dioxole
2.5g
$ 1650.00

Total 6 raw suppliers

Chemical Property of 5-Bromo-6-(chloromethyl)benzo[d][1,3]dioxole

Chemical Property:

Vapor Pressure:0.00102mmHg at 25°C
Boiling Point:311.6°C at 760 mmHg
Flash Point:142.3°C
PSA：18.46000
Density:1.726g/cm³
LogP:2.91660
XLogP3:2.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:247.92397
Heavy Atom Count:12
Complexity:167

Purity/Quality:

98% ^*data from raw suppliers

5-Bromo-6-(chloromethyl)benzo[d][1,3]dioxole 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1OC2=C(O1)C=C(C(=C2)CCl)Br

Technology Process of 5-Bromo-6-(chloromethyl)benzo[d][1,3]dioxole

There total 6 articles about 5-Bromo-6-(chloromethyl)benzo[d][1,3]dioxole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 20850-43-5
5-(chloromethyl)-1,3-benzodioxole

: 64603-67-4
5-bromo-6-(chloromethyl)benzo[d][1,3]dioxole

Guidance literature:: With N-Bromosuccinimide; In acetonitrile; at 20 ℃; for 13h; Inert atmosphere;

Reference yield:

: 495-76-1
piperonol

: 64603-67-4
5-bromo-6-(chloromethyl)benzo[d][1,3]dioxole

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride; triethylamine / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

2: N-Bromosuccinimide / acetonitrile / 13 h / 20 °C / Inert atmosphere

With N-Bromosuccinimide; thionyl chloride; triethylamine; In dichloromethane; acetonitrile;