1-Piperidinecarboxylic acid, 4-[2-[[[2-[[(5-chloro-2-pyridinyl)amino]carbonyl]phenyl]amino]carbonyl]-5 -(1,1-dimethylethyl)phenoxy]-, 1,1-dimethylethyl ester

Base Information

Chemical Name:1-Piperidinecarboxylic acid, 4-[2-[[[2-[[(5-chloro-2-pyridinyl)amino]carbonyl]phenyl]amino]carbonyl]-5 -(1,1-dimethylethyl)phenoxy]-, 1,1-dimethylethyl ester
CAS No.:889120-05-2
Molecular Formula:C33H39ClN4O5
Molecular Weight:607.149
Hs Code.:

1-Piperidinecarboxylic acid,
4-[2-[[[2-[[(5-chloro-2-pyridinyl)amino]carbonyl]phenyl]amino]carbonyl]-5
-(1,1-dimethylethyl)phenoxy]-, 1,1-dimethylethyl ester

Synonyms:

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Chemical Property of 1-Piperidinecarboxylic acid, 4-[2-[[[2-[[(5-chloro-2-pyridinyl)amino]carbonyl]phenyl]amino]carbonyl]-5 -(1,1-dimethylethyl)phenoxy]-, 1,1-dimethylethyl ester

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Technology Process of 1-Piperidinecarboxylic acid, 4-[2-[[[2-[[(5-chloro-2-pyridinyl)amino]carbonyl]phenyl]amino]carbonyl]-5 -(1,1-dimethylethyl)phenoxy]-, 1,1-dimethylethyl ester

There total 11 articles about 1-Piperidinecarboxylic acid, 4-[2-[[[2-[[(5-chloro-2-pyridinyl)amino]carbonyl]phenyl]amino]carbonyl]-5 -(1,1-dimethylethyl)phenoxy]-, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 852370-34-4
2-[1-(tert-butoxycarbonyl)piperidin-4-yloxy]-4-tert-butyl-benzoic acid chloride

: 280771-61-1
N-(5-chloro-2-pyridinyl)(2-amino)phenylcarboxamide

: 889120-05-2
2-{2-[1-(tert-butoxycarbonyl)piperidin-4-yloxy]-4-(tert-butyl)-benzoylamino}-N-(5-chloro-pyridin-2-yl)benzamide

Guidance literature:: With pyridine; In dichloromethane; at 0 - 20 ℃;
DOI:10.1016/j.bmcl.2007.06.051

Reference yield:

: 1072-98-6
5-chloro-2-pyridylamine

: 889120-05-2
2-{2-[1-(tert-butoxycarbonyl)piperidin-4-yloxy]-4-(tert-butyl)-benzoylamino}-N-(5-chloro-pyridin-2-yl)benzamide

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / CH₂Cl₂ / 20 °C

2: H₂ / Raney Ni / tetrahydrofuran; ethyl acetate / 16 h / 20 °C / 3075.31 Torr

3: pyridine / CH₂Cl₂ / 0 - 20 °C

With pyridine; hydrogen; nickel; In tetrahydrofuran; dichloromethane; ethyl acetate;
DOI:10.1016/j.bmcl.2007.06.051

Reference yield:

: 280771-60-0
N-(5-chloropyridine-2-yl)-2-nitrobenzamide

: 889120-05-2
2-{2-[1-(tert-butoxycarbonyl)piperidin-4-yloxy]-4-(tert-butyl)-benzoylamino}-N-(5-chloro-pyridin-2-yl)benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / Raney Ni / tetrahydrofuran; ethyl acetate / 16 h / 20 °C / 3075.31 Torr

2: pyridine / CH₂Cl₂ / 0 - 20 °C

With pyridine; hydrogen; nickel; In tetrahydrofuran; dichloromethane; ethyl acetate;
DOI:10.1016/j.bmcl.2007.06.051