Dithiosalicylide

Base Information

• Chemical Name: Dithiosalicylide
• CAS No.: 21083-38-5
• Molecular Formula: C₁₄H₈O₂S₂
• Molecular Weight: 272.348
• Mol file: 21083-38-5.mol

Synonyms:

Chemical Property of Dithiosalicylide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Dithiosalicylide

There total 1 articles about Dithiosalicylide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methanol (67-56-1) + benzothietan-2-one (21083-36-3) → dibenzo[b,f][1,5]dithiocin-6,12-dione (21083-38-5) + bis[2-(methoxycarbonyl)phenyl]disulfide (5459-63-2) + 1,9,17-trithia-[2.2.2]orthocyclophane-2,10,18-trione (39264-06-7) + Methyl thiosalicylate (4892-02-8)

Guidance literature:

In dichloromethane; at -196 - 20 ℃; for 0.166667h;

DOI:10.1021/jo00226a022

Reference yield:

dibenzo[b,f][1,5]dithiocin-6,12-dione (21083-38-5) → thio-xanthene-9-one (492-22-8)

Guidance literature:

at 200 - 300 ℃;

Reference yield:

dibenzo[b,f][1,5]dithiocin-6,12-dione (21083-38-5) → Thiosalicylic acid (147-93-3)

Guidance literature:

upstream raw materials:

methanol

benzothietan-2-one

Downstream raw materials:

thio-xanthene-9-one

Thiosalicylic acid

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