Benzoic acid, 2-methoxy-, 2-acetyl-4-methylphenyl ester

Base Information

Chemical Name:Benzoic acid, 2-methoxy-, 2-acetyl-4-methylphenyl ester
CAS No.:88951-97-7
Molecular Formula:C17H16O4
Molecular Weight:284.312
Hs Code.:
DSSTox Substance ID:DTXSID50452737
Wikidata:Q82273544

Synonyms:Benzoic acid, 2-methoxy-, 2-acetyl-4-methylphenyl ester;88951-97-7;DTXSID50452737;AKOS005132724

Suppliers and Price of Benzoic acid, 2-methoxy-, 2-acetyl-4-methylphenyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Benzoic acid, 2-methoxy-, 2-acetyl-4-methylphenyl ester

Chemical Property:

XLogP3:3.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:5
Exact Mass:284.10485899
Heavy Atom Count:21
Complexity:379

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=C(C=C1)OC(=O)C2=CC=CC=C2OC)C(=O)C

Technology Process of Benzoic acid, 2-methoxy-, 2-acetyl-4-methylphenyl ester

There total 4 articles about Benzoic acid, 2-methoxy-, 2-acetyl-4-methylphenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1450-72-2
5-methyl-2-hydroxyacetophenone

: 21615-34-9
2-Methoxybenzoyl chloride

: 88951-97-7
2-acetyl-4-methylphenyl 2-methoxybenzoate

Guidance literature:: With pyridine; at 50 ℃; for 0.5h;
DOI:10.1021/jm020839k

Reference yield: 63.0%

: 1450-72-2
5-methyl-2-hydroxyacetophenone

: 579-75-9
2-Methoxybenzoic acid

: 88951-97-7
2-acetyl-4-methylphenyl 2-methoxybenzoate

Guidance literature:: With pyridine; trichlorophosphate; 1) below 5 deg C, 2 h, 2) overnight (ice chest);

Reference yield:

: 106-44-5
p-cresol

: 88951-97-7
2-acetyl-4-methylphenyl 2-methoxybenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine

2: AlCl₃

3: 87 percent / pyridine / 0.5 h / 50 °C

With pyridine; aluminium trichloride; 2: Fries rearrangement / 3: Schotten-Baumann reaction;
DOI:10.1021/jm020839k