2-Propenoic acid, 2-(benzoylamino)-3-(2-thienyl)-, (E)-

Base Information

Chemical Name:2-Propenoic acid, 2-(benzoylamino)-3-(2-thienyl)-, (E)-
CAS No.:88991-20-2
Molecular Formula:C14H11NO3S
Molecular Weight:273.312
Hs Code.:

Synonyms:

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Chemical Property of 2-Propenoic acid, 2-(benzoylamino)-3-(2-thienyl)-, (E)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
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MSDS Files:: SDS file from LookChem

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Technology Process of 2-Propenoic acid, 2-(benzoylamino)-3-(2-thienyl)-, (E)-

There total 5 articles about 2-Propenoic acid, 2-(benzoylamino)-3-(2-thienyl)-, (E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 88991-45-1
(E)-2-Phenyl-5-oxo-4-(2-thienylmethylene)-4,5-dihydro-1,3-oxazole

: 88991-20-2
(E)-2-Benzoylamino-3-(2-thienyl)-2-propenoic acid

Guidance literature:: With sodium hydroxide; In methanol; Ambient temperature;
DOI:10.1055/s-1983-30556

Reference yield:

: 98-03-3
thiophene-2-carbaldehyde

: 88991-20-2
(E)-2-Benzoylamino-3-(2-thienyl)-2-propenoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 57 percent / NaOAc / acetic anhydride / 2 h / 25 °C

2: 0.1 NaOH / 1 h / Heating

With sodium hydroxide; sodium acetate; In acetic anhydride;

Reference yield:

: 495-69-2,140480-84-8,21251-67-2,91787-63-2,66407-11-2
Hippuric Acid

: 88991-20-2
(E)-2-Benzoylamino-3-(2-thienyl)-2-propenoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 79 percent / acetic anhydride, sodium acetate / 2 h / 100 °C

2: 96 percent / 48percent aq. HBr, HBr / 0 °C

3: 47 percent / 1percent aq. NaOH / methanol / Ambient temperature

With sodium hydroxide; hydrogen bromide; sodium acetate; acetic anhydride; In methanol;
DOI:10.1055/s-1983-30556