Trimethyl[1-(4-methylbenzene-1-sulfonyl)prop-2-en-1-yl]silane

Base Information

Chemical Name:Trimethyl[1-(4-methylbenzene-1-sulfonyl)prop-2-en-1-yl]silane
CAS No.:89002-88-0
Molecular Formula:C13H20O2SSi
Molecular Weight:268.452
Hs Code.:
DSSTox Substance ID:DTXSID90553494

Synonyms:89002-88-0;DTXSID90553494;Trimethyl[1-(4-methylbenzene-1-sulfonyl)prop-2-en-1-yl]silane

Suppliers and Price of Trimethyl[1-(4-methylbenzene-1-sulfonyl)prop-2-en-1-yl]silane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of Trimethyl[1-(4-methylbenzene-1-sulfonyl)prop-2-en-1-yl]silane

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:268.09532758
Heavy Atom Count:17
Complexity:354

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)S(=O)(=O)C(C=C)[Si](C)(C)C

Technology Process of Trimethyl[1-(4-methylbenzene-1-sulfonyl)prop-2-en-1-yl]silane

There total 2 articles about Trimethyl[1-(4-methylbenzene-1-sulfonyl)prop-2-en-1-yl]silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 75-77-4
chloro-trimethyl-silane

: 3112-87-6
1-methyl-4-(prop-2-ene-1-sulfonyl)benzene

: 89002-88-0
1-(trimethylsilyl)-1-(p-toluenesulfonyl)-2-propene

Guidance literature:: In tetrahydrofuran; at -78 ℃; 1.) n-butyllithium, hexane, 15 min, 2.) 1 hr.;
DOI:10.1016/S0022-328X(00)98919-8

Reference yield:

: 75-77-4
chloro-trimethyl-silane

: 3112-87-6
1-methyl-4-(prop-2-ene-1-sulfonyl)benzene

: 18000-27-6
trimethylsilyllithium

: 89002-88-0
1-(trimethylsilyl)-1-(p-toluenesulfonyl)-2-propene

Guidance literature:: Yield given. Multistep reaction; 1.) THF-ether, -70 deg C, 30 min; 2.) -70 deg C, 135 min;

Reference yield: 95.0%

: 89002-88-0
1-(trimethylsilyl)-1-(p-toluenesulfonyl)-2-propene

: 98351-37-2
(E)-3-(Toluene-4-sulfonyl)-propenal

Guidance literature:: palladium(II) trifluoroacetate; In acetone; for 38h; Ambient temperature; Irradiation; various catalysts;
DOI:10.1016/S0040-4039(00)61943-3