1-Methyl-4-(1-methylcyclohex-2-ene-1-sulfonyl)benzene

Base Information

Chemical Name:1-Methyl-4-(1-methylcyclohex-2-ene-1-sulfonyl)benzene
CAS No.:89002-90-4
Molecular Formula:C14H18O2S
Molecular Weight:250.362
Hs Code.:
DSSTox Substance ID:DTXSID30541092

Synonyms:89002-90-4;1-Methyl-4-(1-methylcyclohex-2-ene-1-sulfonyl)benzene;DTXSID30541092

Suppliers and Price of 1-Methyl-4-(1-methylcyclohex-2-ene-1-sulfonyl)benzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 1-Methyl-4-(1-methylcyclohex-2-ene-1-sulfonyl)benzene

Chemical Property:

XLogP3:3.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:250.10275099
Heavy Atom Count:17
Complexity:383

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=CC=C(C=C1)S(=O)(=O)C2(CCCC=C2)C

Technology Process of 1-Methyl-4-(1-methylcyclohex-2-ene-1-sulfonyl)benzene

There total 4 articles about 1-Methyl-4-(1-methylcyclohex-2-ene-1-sulfonyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 115125-55-8
3-(p-tolylthio)cyclohexene

: 89002-90-4
1-methyl-1-p-tolylsulphonylcyclohex-2-ene

Guidance literature:: Multi-step reaction with 2 steps

1: 3.62 g / 30 percent hydrogen peroxide, sodium acetate / acetic acid / 50 °C

2: 1.) THF-ether, -70 deg C, 30 min; 2.) -70 deg C, 135 min

With dihydrogen peroxide; sodium acetate; In acetic acid;

Reference yield:

: 1227872-34-5
3-methylcyclohex-2-enyl toluene-p-sulphinate

: 89002-90-4
1-methyl-1-p-tolylsulphonylcyclohex-2-ene

: 89003-00-9
3-methylcyclohex-2-enyl p-tolyl sulphone

Guidance literature:: In formamide; at 55 ℃; for 4h; Yield given. Yields of byproduct given;

Reference yield:

: 10439-23-3
4-methylbenzenesulfinyl chloride

: 89002-90-4
1-methyl-1-p-tolylsulphonylcyclohex-2-ene

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / pyridine / 1.) acetone-solid CO₂ bath, 30 min; 2.) 20 deg C, 30 min

2: formamide / 4 h / 55 °C

In pyridine; formamide;