4-methyl-4-p-tolylsulphonylcyclohex-2-enyl (3'-p-tolylsulphonyl)propionate

Base Information

Chemical Name:4-methyl-4-p-tolylsulphonylcyclohex-2-enyl (3'-p-tolylsulphonyl)propionate
CAS No.:120801-59-4
Molecular Formula:C₂₄H₂₈O₆S₂
Molecular Weight:476.615
Hs Code.:

Synonyms:4-methyl-4-p-tolylsulphonylcyclohex-2-enyl (3'-p-tolylsulphonyl)propionate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-methyl-4-p-tolylsulphonylcyclohex-2-enyl (3'-p-tolylsulphonyl)propionate

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Technology Process of 4-methyl-4-p-tolylsulphonylcyclohex-2-enyl (3'-p-tolylsulphonyl)propionate

There total 4 articles about 4-methyl-4-p-tolylsulphonylcyclohex-2-enyl (3'-p-tolylsulphonyl)propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 120801-50-5,120801-51-6
4-methyl-4-p-tolylsulphonylcyclohex-2-enyl acrylate

: 120801-59-4
4-methyl-4-p-tolylsulphonylcyclohex-2-enyl (3'-p-tolylsulphonyl)propionate

Guidance literature:: With sodium 4-methylbenzenesulfinate; In acetic acid; at 100 ℃; for 16h;

Reference yield: 89.0%

: 120801-52-7,120801-53-8
4-methyl-4-p-tolylsulphonylcyclohex-2-enyl 2'-trimethylsilylacrylate

: 120801-59-4
4-methyl-4-p-tolylsulphonylcyclohex-2-enyl (3'-p-tolylsulphonyl)propionate

Guidance literature:: With sodium 4-methylbenzenesulfinate; In acetic acid; at 100 ℃; for 16h;

Reference yield:

: 89002-90-4
1-methyl-1-p-tolylsulphonylcyclohex-2-ene

: 120801-59-4
4-methyl-4-p-tolylsulphonylcyclohex-2-enyl (3'-p-tolylsulphonyl)propionate

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / N-bromosuccinimide, dibenzoyl peroxide / CCl₄ / 4 h / Heating

2: 29 percent / dimethylformamide / 16 h / 100 °C

3: 94 percent / sodium p-tolylsulphinate / aq. acetic acid / 16 h / 100 °C

With N-Bromosuccinimide; sodium 4-methylbenzenesulfinate; dibenzoyl peroxide; In tetrachloromethane; acetic acid; N,N-dimethyl-formamide;