3-(Phenylsulfanyl)prop-2-yn-1-ol

Base Information

Chemical Name:3-(Phenylsulfanyl)prop-2-yn-1-ol
CAS No.:89005-19-6
Molecular Formula:C9H8OS
Molecular Weight:164.228
Hs Code.:
DSSTox Substance ID:DTXSID60563767
Nikkaji Number:J622.302H
Wikidata:Q82448248

Synonyms:89005-19-6;3-(Phenylsulfanyl)prop-2-yn-1-ol;DTXSID60563767

Suppliers and Price of 3-(Phenylsulfanyl)prop-2-yn-1-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 3-(Phenylsulfanyl)prop-2-yn-1-ol

Chemical Property:

XLogP3:2.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:164.02958605
Heavy Atom Count:11
Complexity:159

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)SC#CCO

Technology Process of 3-(Phenylsulfanyl)prop-2-yn-1-ol

There total 9 articles about 3-(Phenylsulfanyl)prop-2-yn-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 107-19-7
propargyl alcohol

: 882-33-7
diphenyldisulfane

: 89005-19-6
3-(phenylsulfanyl)propargyl alcohol

Guidance literature:: With potassium phosphate; copper(l) iodide; 2,6-bis(2'-pyridyl)-4-(p-methoxyphenyl)pyridine; In dimethyl sulfoxide; at 50 ℃; for 7h;
DOI:10.1055/s-0033-1341277

Reference yield: 50.0%

: 1212-08-4
S-Phenyl benzenethiosulfonate

: 107-19-7
propargyl alcohol

: 89005-19-6
3-(phenylsulfanyl)propargyl alcohol

Guidance literature:: propargyl alcohol; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1h;

S-Phenyl benzenethiosulfonate; In tetrahydrofuran; hexane; at -50 - -20 ℃; for 2h;
DOI:10.1002/ejoc.201402577

Reference yield:

: 107-19-7
propargyl alcohol

: 882-33-7
diphenyldisulfane

: 100-68-5
methyl-phenyl-thioether

: 89005-19-6
3-(phenylsulfanyl)propargyl alcohol

Guidance literature:: With n-butyllithium; methyl iodide; Yield given. Multistep reaction. Yields of byproduct given; 1.) THF, -30 deg C, 30 min, 2.) THF, r.t, 1 h;