Technology Process of 3-Benzyl-2,5-dimethoxy-2,4-dimethyl-2,5-dihydrofuran
There total 3 articles about 3-Benzyl-2,5-dimethoxy-2,4-dimethyl-2,5-dihydrofuran which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetraethylammonium perchlorate;
for 4h;
Ambient temperature;
platinum foil electrodes (18.7 mA/cm2);
DOI:10.1055/s-1983-30598
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 80 percent / m-perbenzoic acid / CH2Cl2 / 12 h
2: 67 percent / HCl / methanol / 6 h / 65 °C
3: 85 percent / tetraethylammonium perchlorate / 4 h / Ambient temperature; platinum foil electrodes (18.7 mA/cm2)
With
hydrogenchloride; m-perbenzoic acid; tetraethylammonium perchlorate;
In
methanol; dichloromethane;
DOI:10.1055/s-1983-30598
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 67 percent / HCl / methanol / 6 h / 65 °C
2: 85 percent / tetraethylammonium perchlorate / 4 h / Ambient temperature; platinum foil electrodes (18.7 mA/cm2)
With
hydrogenchloride; tetraethylammonium perchlorate;
In
methanol;
DOI:10.1055/s-1983-30598
