3-Benzyl-2,5-dimethoxy-2,4-dimethyl-2,5-dihydrofuran

Base Information

Chemical Name:3-Benzyl-2,5-dimethoxy-2,4-dimethyl-2,5-dihydrofuran
CAS No.:89100-10-7
Molecular Formula:C₁₅H₂₀O₃
Molecular Weight:248.322
Hs Code.:
DSSTox Substance ID:DTXSID60527940

Synonyms:89100-10-7;3-Benzyl-2,5-dimethoxy-2,4-dimethyl-2,5-dihydrofuran;DTXSID60527940

Suppliers and Price of 3-Benzyl-2,5-dimethoxy-2,4-dimethyl-2,5-dihydrofuran

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 3-Benzyl-2,5-dimethoxy-2,4-dimethyl-2,5-dihydrofuran

Chemical Property:

XLogP3:1.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:248.14124450
Heavy Atom Count:18
Complexity:318

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=C(C(OC1OC)(C)OC)CC2=CC=CC=C2

Technology Process of 3-Benzyl-2,5-dimethoxy-2,4-dimethyl-2,5-dihydrofuran

There total 3 articles about 3-Benzyl-2,5-dimethoxy-2,4-dimethyl-2,5-dihydrofuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 67-56-1
methanol

: 89100-08-3
3-Benzyl-2,4-dimethylfuran

: 89100-10-7
3-Benzyl-2,5-dimethoxy-2,4-dimethyl-2,5-dihydrofuran

Guidance literature:: With tetraethylammonium perchlorate; for 4h; Ambient temperature; platinum foil electrodes (18.7 mA/cm²);
DOI:10.1055/s-1983-30598

Reference yield:

: 67935-53-9
3-Benzyl-4-methyl-4-penten-2-one

: 89100-10-7
3-Benzyl-2,5-dimethoxy-2,4-dimethyl-2,5-dihydrofuran

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / m-perbenzoic acid / CH₂Cl₂ / 12 h

2: 67 percent / HCl / methanol / 6 h / 65 °C

3: 85 percent / tetraethylammonium perchlorate / 4 h / Ambient temperature; platinum foil electrodes (18.7 mA/cm²)

With hydrogenchloride; m-perbenzoic acid; tetraethylammonium perchlorate; In methanol; dichloromethane;
DOI:10.1055/s-1983-30598

Reference yield:

: 89100-04-9
3-Benzyl-4-methyl-4,5-epoxy-2-pentenone

: 89100-10-7
3-Benzyl-2,5-dimethoxy-2,4-dimethyl-2,5-dihydrofuran

Guidance literature:: Multi-step reaction with 2 steps

1: 67 percent / HCl / methanol / 6 h / 65 °C

2: 85 percent / tetraethylammonium perchlorate / 4 h / Ambient temperature; platinum foil electrodes (18.7 mA/cm²)

With hydrogenchloride; tetraethylammonium perchlorate; In methanol;
DOI:10.1055/s-1983-30598