2-Methoxy-1-phenyl-2-(phenylsulfanyl)ethan-1-one

Base Information

Chemical Name:2-Methoxy-1-phenyl-2-(phenylsulfanyl)ethan-1-one
CAS No.:89171-35-7
Molecular Formula:C15H14O2S
Molecular Weight:258.341
Hs Code.:
DSSTox Substance ID:DTXSID60513383

Synonyms:89171-35-7;2-Methoxy-1-phenyl-2-(phenylsulfanyl)ethan-1-one;DTXSID60513383;2-methoxy-1-phenyl-2-phenylsulfanylethanone;2-methoxy-1-phenyl-2-(phenylsulfanyl)ethanone

Suppliers and Price of 2-Methoxy-1-phenyl-2-(phenylsulfanyl)ethan-1-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Methoxy-1-phenyl-2-(phenylsulfanyl)ethan-1-one

Chemical Property:

XLogP3:3.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:5
Exact Mass:258.07145086
Heavy Atom Count:18
Complexity:255

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC(C(=O)C1=CC=CC=C1)SC2=CC=CC=C2

Technology Process of 2-Methoxy-1-phenyl-2-(phenylsulfanyl)ethan-1-one

There total 7 articles about 2-Methoxy-1-phenyl-2-(phenylsulfanyl)ethan-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 67-56-1
methanol

: 67655-17-8
α-chloro-α-(phenylthio)acetophenone

: 89171-35-7
2‐methoxy‐1‐phenyl‐2‐(phenylsulfanyl) ethanone

Guidance literature:: at 15 ℃;
DOI:10.1016/S0040-4039(00)87185-3

Reference yield: 94.0%

: 13865-50-4
methoxymethyl phenyl sulfide

: 611-74-5
N,N-dimethylbenzamide

: 89171-35-7
2‐methoxy‐1‐phenyl‐2‐(phenylsulfanyl) ethanone

Guidance literature:: With tert.-butyl lithium; 1.) THF-pentane, -78 deg C, 2 h, 2.) -> RT, 1 h;

Reference yield: 88.0%

: 6919-61-5
N-methoxy-N-methylbenzamide

: 13865-50-4
methoxymethyl phenyl sulfide

: 89171-35-7
2‐methoxy‐1‐phenyl‐2‐(phenylsulfanyl) ethanone

Guidance literature:: methoxymethyl phenyl sulfide; With 1,4-diaza-bicyclo[2.2.2]octane; n-butyllithium; In tetrahydrofuran; hexane; at -78 - -40 ℃; for 1.5h; Inert atmosphere;

N-methoxy-N-methylbenzamide; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 18h; chemoselective reaction; Inert atmosphere;
DOI:10.1002/ejoc.201800095