1-(Diazomethyl)-1-methyl-2,3,4,5-tetraphenyl-1H-silole

Base Information

• Chemical Name: 1-(Diazomethyl)-1-methyl-2,3,4,5-tetraphenyl-1H-silole
• CAS No.: 89175-80-4
• Molecular Formula: C₃₀H₂₄N₂Si
• Molecular Weight: 440.619
• DSSTox Substance ID: DTXSID00525142

Synonyms:89175-80-4;DTXSID00525142;1-(Diazomethyl)-1-methyl-2,3,4,5-tetraphenyl-1H-silole

Chemical Property of 1-(Diazomethyl)-1-methyl-2,3,4,5-tetraphenyl-1H-silole

Chemical Property:

• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 5
• Exact Mass: 440.170875308
• Heavy Atom Count: 33
• Complexity: 737

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C[Si]1(C(=C(C(=C1C2=CC=CC=C2)C3=CC=CC=C3)C4=CC=CC=C4)C5=CC=CC=C5)C=[N+]=[N-]

Technology Process of 1-(Diazomethyl)-1-methyl-2,3,4,5-tetraphenyl-1H-silole

There total 1 articles about 1-(Diazomethyl)-1-methyl-2,3,4,5-tetraphenyl-1H-silole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-chloromethyl-1-methyl-2,3,4,5-tetraphenyl-1-silacyclopentadiene (94671-34-8) → 1-methyl-2,3,4,5-tetraphenylsilacyclopentadienyl-diazomethane (89175-80-4)

Guidance literature:

With diphenylphosphoranyl azide; magnesium; Yield given. Multistep reaction; 1) THF, 2) 0 deg C;

DOI:10.1016/S0040-4039(00)88312-4

Reference yield: 64.0%

1-methyl-2,3,4,5-tetraphenylsilacyclopentadienyl-diazomethane (89175-80-4) → 1-methyl-2,3,4,5-tetraphenylsilacyclopentadienyl-diazirine (89175-81-5)

Guidance literature:

In benzene; Irradiation;

DOI:10.1016/S0040-4039(00)88312-4

Reference yield: 48.0%

methanol (67-56-1) + 1-methyl-2,3,4,5-tetraphenylsilacyclopentadienyl-diazomethane (89175-80-4) → 1-Methoxy-1-methyl-2,3,4,5-tetraphenyl-1,4-dihydro-siline (89175-83-7) + 1-Methoxy-1-methyl-3,4,5,6-tetraphenyl-1,2-dihydro-siline (89175-85-9) + 1-Ethyl-1-methoxy-2,3,4,5-tetraphenyl-1H-silole (89175-86-0) + 1-methyl-2,3,4,5-tetraphenylsilacyclopentadienyl-diazirine (89175-81-5)

Guidance literature:

In benzene; Irradiation;

DOI:10.1016/S0040-4039(00)88312-4

upstream raw materials:

1-chloromethyl-1-methyl-2,3,4,5-tetraphenyl-1-silacyclopentadiene

Downstream raw materials:

1-Methoxy-1-methyl-2,3,4,5-tetraphenyl-1,4-dihydro-siline

1-Methoxy-1-methyl-3,4,5,6-tetraphenyl-1,2-dihydro-siline

1-Ethyl-1-methoxy-2,3,4,5-tetraphenyl-1H-silole

1-methyl-2,3,4,5-tetraphenylsilacyclopentadienyl-diazirine

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