Silanamine, N-(4-bromophenyl)-N,1,1,1-tetramethyl-

Base Information

Chemical Name:Silanamine, N-(4-bromophenyl)-N,1,1,1-tetramethyl-
CAS No.:89232-80-4
Molecular Formula:C10H16BrNSi
Molecular Weight:258.233
Hs Code.:
DSSTox Substance ID:DTXSID20579304
Wikidata:Q82469790

Synonyms:89232-80-4;Silanamine, N-(4-bromophenyl)-N,1,1,1-tetramethyl-;N-(4-Bromophenyl)-N,1,1,1-tetramethylsilanamine;SCHEMBL10598345;DTXSID20579304;4-bromo-N-methyl-N-trimethylsilylaniline

Suppliers and Price of Silanamine, N-(4-bromophenyl)-N,1,1,1-tetramethyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Silanamine, N-(4-bromophenyl)-N,1,1,1-tetramethyl-

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:257.02354
Heavy Atom Count:13
Complexity:159

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN(C1=CC=C(C=C1)Br)[Si](C)(C)C

Technology Process of Silanamine, N-(4-bromophenyl)-N,1,1,1-tetramethyl-

There total 4 articles about Silanamine, N-(4-bromophenyl)-N,1,1,1-tetramethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 75-77-4
chloro-trimethyl-silane

: 6911-87-1,211060-12-7
4-bromo-N-methylaniline

: 89232-80-4
4-bromo-N-methyl-N-trimethylsilylaniline

Guidance literature:: 4-bromo-N-methylaniline; With n-butyllithium; In tetrahydrofuran; hexane; at 0 - 20 ℃; for 1h;

chloro-trimethyl-silane; In tetrahydrofuran; hexane; at 20 ℃;
DOI:10.1021/tx0256679

Reference yield:

: 6911-87-1,211060-12-7
4-bromo-N-methylaniline

: 89232-80-4
4-bromo-N-methyl-N-trimethylsilylaniline

Guidance literature:: With n-butyllithium; diisopropylamine; In tetrahydrofuran; hexane;

Reference yield:

: 100-61-8
N-methylaniline

: 89232-80-4
4-bromo-N-methyl-N-trimethylsilylaniline

Guidance literature:: Multi-step reaction with 2 steps

1.1: 99 percent / tetrabromo-2,5-cyclohexadienone / CH₂Cl₂ / 2 h / -78 - 20 °C

2.1: butyllithium / hexane; tetrahydrofuran / 1 h / 0 - 20 °C

2.2: 66 percent / hexane; tetrahydrofuran / 20 °C

With n-butyllithium; 2,4,4,6-Tetrabromo-2,5-cyclohexadien-1-one; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1021/tx0256679