iodoaluminum(2+) dimethanide

Base Information

• Chemical Name: iodoaluminum(2+) dimethanide
• CAS No.: 2938-72-9
• Molecular Formula: C2H6 Al I
• Molecular Weight: 183.956
• Mol file: 2938-72-9.mol

Synonyms:Dimethylaluminumiodide (6CI); Iododimethylaluminum

Chemical Property of iodoaluminum(2+) dimethanide

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• PSA: 0.00000
• Density: g/cm³
• LogP: -1.75790

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of iodoaluminum(2+) dimethanide

There total 2 articles about iodoaluminum(2+) dimethanide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

triethylaluminum (97-93-8) + aluminium (7429-90-5) → trimethylaluminum (75-24-1) + dimethyl aluminum iodide (2938-72-9)

Guidance literature:

With iodine; methyl iodide; In ethanol; Sonication; N2, CH3I, I2 and Al introduced in a condenser with C2H5OH at -20°C, ultrasonic acceleration at room temp. for 2 h, Et3Al (ratio MeI/Et3Al = 3.00) dropped into soln. within 10 min, sonicated for 30 min; distilled (vac.);

DOI:10.1016/S0022-328X(00)98951-4

Reference yield: 62.5%

triethylaluminum (97-93-8) + aluminium (7429-90-5) → trimethylaluminum (75-24-1) + dimethyl aluminum iodide (2938-72-9) + ethyl aluminium iodide (2938-73-0)

Guidance literature:

With iodine; methyl iodide; In ethanol; Sonication; N2, CH3I, I2 and Al introduced in a condenser with C2H5OH at -20°C, ultrasonic acceleration at room temp. for 2 h, Et3Al (ratio MeI/Et3Al = 12.00) dropped into soln. within 10 min, sonicated for 30 min; distilled (vac.);

DOI:10.1016/S0022-328X(00)98951-4

Reference yield:

dimethyl aluminum iodide (2938-72-9) + methoxybenzene (100-66-3) → dimethylaluminum phenoxide (6062-74-4)

Guidance literature:

at 135 ℃; for 6h; Rate constant; var. temp.;

DOI:10.1016/S0022-328X(00)99359-8

upstream raw materials:

triethylaluminum

aluminium

Downstream raw materials:

dimethylaluminum phenoxide

Refernces