Technology Process of 2-Oxo-1,4-diphenylbutyl acetate
There total 3 articles about 2-Oxo-1,4-diphenylbutyl acetate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
2-(4-methoxyphenyl)-6,7-dihydro-5H-pyrrolo[2,1-c][1,2,4]triazol-2-ium tetrafluoroborate; potassium carbonate;
In
tetrahydrofuran;
for 24h;
Inert atmosphere;
Reflux;
DOI:10.1021/acs.orglett.1c01134
- Guidance literature:
-
Multi-step reaction with 2 steps
1: toluene-4-sulfonic acid / 20 °C / Inert atmosphere
2: potassium carbonate; 2-(4-methoxyphenyl)-6,7-dihydro-5H-pyrrolo[2,1-c][1,2,4]triazol-2-ium tetrafluoroborate / tetrahydrofuran / 24 h / Inert atmosphere; Reflux
With
2-(4-methoxyphenyl)-6,7-dihydro-5H-pyrrolo[2,1-c][1,2,4]triazol-2-ium tetrafluoroborate; potassium carbonate; toluene-4-sulfonic acid;
In
tetrahydrofuran;
DOI:10.1021/acs.orglett.1c01134
- Guidance literature:
-
With
1-chloro-1-(dimethylamino)-2-methyl-1-propene;
copper(l) iodide;
Yield given. Multistep reaction;
1.) THF, dichloromethane, 0 deg C, 3 h; 2.) 0 deg C, 1 h;
DOI:10.1246/cl.1983.1791
