N-[(4-Methylbenzene-1-sulfonyl)oxy]-P,P-diphenylphosphinic amide

Base Information

Chemical Name:N-[(4-Methylbenzene-1-sulfonyl)oxy]-P,P-diphenylphosphinic amide
CAS No.:89267-63-0
Molecular Formula:C₁₉H₁₈NO₄PS
Molecular Weight:387.396
Hs Code.:
DSSTox Substance ID:DTXSID20525785
Wikidata:Q82393633

Synonyms:89267-63-0;DTXSID20525785;N-[(4-Methylbenzene-1-sulfonyl)oxy]-P,P-diphenylphosphinic amide

Suppliers and Price of N-[(4-Methylbenzene-1-sulfonyl)oxy]-P,P-diphenylphosphinic amide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of N-[(4-Methylbenzene-1-sulfonyl)oxy]-P,P-diphenylphosphinic amide

Chemical Property:

XLogP3:3.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:6
Exact Mass:387.06941623
Heavy Atom Count:26
Complexity:561

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)S(=O)(=O)ONP(=O)(C2=CC=CC=C2)C3=CC=CC=C3

Technology Process of N-[(4-Methylbenzene-1-sulfonyl)oxy]-P,P-diphenylphosphinic amide

There total 2 articles about N-[(4-Methylbenzene-1-sulfonyl)oxy]-P,P-diphenylphosphinic amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 73452-52-5
N-hydroxy-P,P-diphenylphosphinic amide

: 98-59-9
p-toluenesulfonyl chloride

: 89267-63-0
N-(diphenylphosphinoyl)-O-(p-tolylsulphonyl)hydroxylamine

Guidance literature:: With pyridine; for 1.8h; Ambient temperature;

Reference yield:

: 1499-21-4
Diphenylphosphinic chloride

: 89267-63-0
N-(diphenylphosphinoyl)-O-(p-tolylsulphonyl)hydroxylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) trimethylsilylhydroxylamine, triethylamine, 2.) methanol / 1.) dichloromethane, 1.6 h, RT, 2.) 3 h

2: 42 percent / pyridine / 1.8 h / Ambient temperature

With pyridine; methanol; trimethylsilylhydroxylamine; triethylamine;