N-(Hex-5-en-1-yl)-1,1,1-trimethyl-N-(trimethylsilyl)silanamine

Base Information

• Chemical Name: N-(Hex-5-en-1-yl)-1,1,1-trimethyl-N-(trimethylsilyl)silanamine
• CAS No.: 89333-68-6
• Molecular Formula: C12H29NSi2
• Molecular Weight: 243.54
• DSSTox Substance ID: DTXSID70518647
• Nikkaji Number: J3.511.784I
• Wikidata: Q82381415
• Mol file: 89333-68-6.mol

Synonyms:89333-68-6;N,N-bis(trimethylsilyl)hex-5-en-1-amine;N-(Hex-5-en-1-yl)-1,1,1-trimethyl-N-(trimethylsilyl)silanamine;DTXSID70518647

Chemical Property of N-(Hex-5-en-1-yl)-1,1,1-trimethyl-N-(trimethylsilyl)silanamine

Chemical Property:

• PSA: 3.24000
• LogP: 4.31450
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 7
• Exact Mass: 243.18385300
• Heavy Atom Count: 15
• Complexity: 175

Purity/Quality:

99.3% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C[Si](C)(C)N(CCCCC=C)[Si](C)(C)C

Technology Process of N-(Hex-5-en-1-yl)-1,1,1-trimethyl-N-(trimethylsilyl)silanamine

There total 2 articles about N-(Hex-5-en-1-yl)-1,1,1-trimethyl-N-(trimethylsilyl)silanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

N-(methoxymethyl)-1,1,1-trimethyl-N-(trimethylsilyl)silanamine (88211-44-3) + bromopentene (1119-51-3) → 6-bis(trimethylsilyl)amino-1-hexene (89333-68-6)

Guidance literature:

bromopentene; With magnesium; In diethyl ether; Reflux;

N-(methoxymethyl)-1,1,1-trimethyl-N-(trimethylsilyl)silanamine; In diethyl ether; at 20 ℃; for 4h;

DOI:10.1021/ma200836d

Reference yield: 73.0%

4-penten-1-ylmagnesium bromide (34164-50-6) + N-(methoxymethyl)-1,1,1-trimethyl-N-(trimethylsilyl)silanamine (88211-44-3) → 6-bis(trimethylsilyl)amino-1-hexene (89333-68-6)

Guidance literature:

In diethyl ether; at 20 ℃; for 2h;

DOI:10.1039/c5ta09949h

Reference yield:

6-bis(trimethylsilyl)amino-1-hexene (89333-68-6) → 1,6-Hexanediamine (124-09-4)

Guidance literature:

With sodium hypochlorite; dimethylborane; ammonia; Yield given. Multistep reaction; 1.) 0 deg C, 1 h, 2.) O deg C;

upstream raw materials:

N-(methoxymethyl)-1,1,1-trimethyl-N-(trimethylsilyl)silanamine

bromopentene

4-penten-1-ylmagnesium bromide

Downstream raw materials:

1,6-Hexanediamine

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