N,N-Di(propan-2-yl)-2,3-dihydro-1H-borol-1-amine

Base Information

Chemical Name:N,N-Di(propan-2-yl)-2,3-dihydro-1H-borol-1-amine
CAS No.:89377-14-0
Molecular Formula:C₁₀H₂₀BN
Molecular Weight:165.087
Hs Code.:
DSSTox Substance ID:DTXSID30525059
Nikkaji Number:J3.334.001J
Wikidata:Q82392378

Synonyms:89377-14-0;N,N-Di(propan-2-yl)-2,3-dihydro-1H-borol-1-amine;DTXSID30525059

Suppliers and Price of N,N-Di(propan-2-yl)-2,3-dihydro-1H-borol-1-amine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of N,N-Di(propan-2-yl)-2,3-dihydro-1H-borol-1-amine

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:165.1688798
Heavy Atom Count:12
Complexity:155

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:B1(CCC=C1)N(C(C)C)C(C)C

Technology Process of N,N-Di(propan-2-yl)-2,3-dihydro-1H-borol-1-amine

There total 1 articles about N,N-Di(propan-2-yl)-2,3-dihydro-1H-borol-1-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1617500-33-0
C₂₂H₂₁B₂F₁₀N

: 100-52-7
benzaldehyde

: 89377-14-0
1-(diisopropylamino)-2,3-dihydroborole

: 1617500-35-2
C₁₉H₇BF₁₀O

Guidance literature:: In benzene-d6; Inert atmosphere;
DOI:10.1039/c4dt01423e

Reference yield: 75.0%

: 89377-14-0
1-(diisopropylamino)-2,3-dihydroborole

: 591-51-5
phenyllithium

: 89377-15-1
1-phenyl-2-borolene

Guidance literature:: With hydrogenchloride; In diethyl ether; byproducts: {NH2(iPr)2}Cl; (N2) or (Ar); addn. of LiPh to 1-(diisopropylamino)-2-borolene at -10°C; kept for 1 h at room temp.; dropwise addn. of HCl (Et2O) at -80°C under vigorously stirring; filtration; removal of solvent in vac.; condensation of residue at E-6 bar;