Methyl 13-hydroxytridecanoate

Base Information

Chemical Name:Methyl 13-hydroxytridecanoate
CAS No.:7147-29-7
Molecular Formula:C14H28O3
Molecular Weight:244.3703
Hs Code.:
NSC Number:28480
DSSTox Substance ID:DTXSID90282858
Nikkaji Number:J297.429K
Wikidata:Q82017235

Synonyms:methyl 13-hydroxytridecanoate;7147-29-7;NSC28480;SCHEMBL1193831;DTXSID90282858;NSC-28480;F79849

Suppliers and Price of Methyl 13-hydroxytridecanoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of Methyl 13-hydroxytridecanoate

Chemical Property:

Vapor Pressure:1.48E-05mmHg at 25°C
Boiling Point:327.8°C at 760 mmHg
Flash Point:123.6°C
Density:0.937g/cm³
XLogP3:4.2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:13
Exact Mass:244.20384475
Heavy Atom Count:17
Complexity:169

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC(=O)CCCCCCCCCCCCO

Technology Process of Methyl 13-hydroxytridecanoate

There total 13 articles about Methyl 13-hydroxytridecanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 3927-59-1
tridecanedioic acid monomethyl ester

: 13362-52-2
1,13-tridecanediol

: 7147-29-7
methyl ω-hydroxytridecanoate

Guidance literature:: With water; Rh₆(CO)16*Mo(CO)6; In 1,2-dimethoxyethane; at 160 ℃; for 16h; under 76000 Torr;
DOI:10.1016/0040-4039(94)02453-I

Reference yield: 47.5%

: 67-56-1
methanol

: 88229-67-8
12-(5,5-Dimethyl-4,5-dihydro-oxazol-2-yl)-dodecan-1-ol

: 7147-29-7
methyl ω-hydroxytridecanoate

Guidance literature:: With sulfuric acid; for 18h; Heating;
DOI:10.1021/jo00179a023

Reference yield:

: 112-86-7
cis-13-docosenoic acid

: 7147-29-7
methyl ω-hydroxytridecanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: O₃ / ethanol; cyclohexane / 4 h / 0 - 5 °C

1.2: KBH₄ / methanol / 8 h / 0 °C

2.1: 16.3 g / SOCl₂ / 1 h / 0 °C

With thionyl chloride; ozone; In ethanol; cyclohexane;
DOI:10.1002/chem.200390021