2-(Phenylmethoxymethyl)oxan-3-ol

Base Information

Chemical Name:2-(Phenylmethoxymethyl)oxan-3-ol
CAS No.:89429-83-4
Molecular Formula:C₁₃H₁₈O₃
Molecular Weight:222.284
Hs Code.:
DSSTox Substance ID:DTXSID00553783

Synonyms:89429-83-4;SCHEMBL7293795;DTXSID00553783;1,5-Anhydro-6-O-benzyl-2,3-dideoxyhexitol

Suppliers and Price of 2-(Phenylmethoxymethyl)oxan-3-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 2-(Phenylmethoxymethyl)oxan-3-ol

Chemical Property:

XLogP3:1.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:222.125594432
Heavy Atom Count:16
Complexity:190

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1CC(C(OC1)COCC2=CC=CC=C2)O

Technology Process of 2-(Phenylmethoxymethyl)oxan-3-ol

There total 13 articles about 2-(Phenylmethoxymethyl)oxan-3-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 89429-82-3
6-benzyloxymethyl-3,4-dihydro-2H-pyran

: 89429-83-4
hydroxy-3 benzyloxymethyl-2 tetrahydropyranne

Guidance literature:: With ;; borane;

Reference yield:

: 107757-68-6
dl-2-benzyloxymethyltetrahydropyran-3-one

: 89429-83-4,104954-94-1,104975-67-9
dl-cis-2-benzyloxymethyltetrahydropyran-3-ol

Guidance literature:: With L-Selectride; In tetrahydrofuran; Yield given; 1.) 5 deg C, 30 min, 2.) room temp., 2 h;
DOI:10.1248/cpb.37.2379

Reference yield:

: 100-44-7
benzyl chloride

: 89429-83-4,104954-94-1,104975-67-9
dl-cis-2-benzyloxymethyltetrahydropyran-3-ol

Guidance literature:: Multi-step reaction with 4 steps

1: 92 percent / 55percent NaH / dimethylformamide / 16 h / Ambient temperature

2: 1.) 1M BH₃, 2.) 10percent aq. NaOH, 30percent aq. H₂O₂ / 1.) THF, room temp., 3 h, 2.) THF, H₂O, room temp., 1 h

3: 2.08 g / CrO₃ / acetone / 1 h / Ambient temperature

4: L-Selectride / tetrahydrofuran / 1.) 5 deg C, 30 min, 2.) room temp., 2 h

With chromium(VI) oxide; sodium hydroxide; borane; dihydrogen peroxide; L-Selectride; sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide; acetone;
DOI:10.1248/cpb.37.2379