N-(9H-fluoren-9-yl)-2,2,2-trifluoro-acetamide

Base Information

Chemical Name:N-(9H-fluoren-9-yl)-2,2,2-trifluoro-acetamide
CAS No.:1493-54-5
Molecular Formula:C₁₅H₁₀F₃NO
Molecular Weight:277.246
Hs Code.:2924299090
Mol file:1493-54-5.mol

Synonyms:Acetamide,N-fluoren-9-yl-2,2,2-trifluoro- (6CI,8CI);NSC 57445;n-(9H-Fluoren-9-yl)-2,2,2-trifluoroacetamide;AC1L6FZ2;AC1Q4I7F;NCIOpen2_002453;MolPort-001-824-091;AR-1J9744;CID245480;

Suppliers and Price of N-(9H-fluoren-9-yl)-2,2,2-trifluoro-acetamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
9-(2,2,2-TRIFLUOROACETAMIDO)FLUORENE Aldrich
1ea
$ 57.00

American Custom Chemicals Corporation
9-(2,2,2-TRIFLUOROACETAMIDO)FLUORENE 95.00%
5MG
$ 504.57

Total 12 raw suppliers

Chemical Property of N-(9H-fluoren-9-yl)-2,2,2-trifluoro-acetamide

Chemical Property:

Vapor Pressure:5.91E-07mmHg at 25°C
Refractive Index:1.585
Boiling Point:410.7 °C at 760 mmHg
Flash Point:202.2 °C
PSA：29.10000
Density:1.37 g/cm³
LogP:3.82580

Purity/Quality:

98%,99%, ^*data from raw suppliers

9-(2,2,2-TRIFLUOROACETAMIDO)FLUORENE Aldrich ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of N-(9H-fluoren-9-yl)-2,2,2-trifluoro-acetamide

There total 2 articles about N-(9H-fluoren-9-yl)-2,2,2-trifluoro-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 525-03-1
9-aminofluorene

: 407-25-0
trifluoroacetic anhydride

: 1493-54-5
N-(9-fluorenyl)trifluoroacetamide

Guidance literature:: In diethyl ether; for 1h;
DOI:10.1021/jm980440p

Reference yield:

: 1493-54-5
N-(9-fluorenyl)trifluoroacetamide

Guidance literature:: 9-Amino-fluoren-hydrochlorid, Trifluoracetanhydrid, Py., zuletzt Δ (Dampfbad);
DOI:10.1021/jo01351a023

Reference yield:

: 1493-54-5
N-(9-fluorenyl)trifluoroacetamide

: 2-(3,4-dimethoxy-phenyl)-6-[(9H-fluoren-9-yl)-methyl-amino]-2-isopropyl-hex-4-ynenitrile

Guidance literature:: Multi-step reaction with 2 steps

1: 2.) KOH / 1.) acetone, 30 min, 2.) 80 deg C, 8 h

2: CuSO₄ / ethanol; H₂O / 16 h / Heating

With potassium hydroxide; copper(II) sulfate; In ethanol; water;
DOI:10.1021/jm980440p