N-methyl-9H-fluoren-9-amine

Base Information

Chemical Name:N-methyl-9H-fluoren-9-amine
CAS No.:38359-28-3
Molecular Formula:C14H13N
Molecular Weight:195.26000
Hs Code.:
DSSTox Substance ID:DTXSID50588308
Wikidata:Q82480905
Mol file:38359-28-3.mol

Synonyms:N-methyl-9H-fluoren-9-amine;38359-28-3;FLUOREN-9-YL-METHYLAMINE;SCHEMBL6998428;DTXSID50588308;AKOS000132225;MCULE-5141181329;CS-0265482;EN300-98875;G49527;Z44508054

Suppliers and Price of N-methyl-9H-fluoren-9-amine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
N-methyl-9H-fluoren-9-amine
10mg
$ 45.00

AK Scientific
N-Methyl-9H-fluoren-9-amine
1g
$ 754.00

Total 2 raw suppliers

Chemical Property of N-methyl-9H-fluoren-9-amine

Chemical Property:

PSA：12.03000
LogP:3.36670
XLogP3:2.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:195.104799419
Heavy Atom Count:15
Complexity:203

Purity/Quality:

99% ^*data from raw suppliers

N-methyl-9H-fluoren-9-amine ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CNC1C2=CC=CC=C2C3=CC=CC=C13

Technology Process of N-methyl-9H-fluoren-9-amine

There total 8 articles about N-methyl-9H-fluoren-9-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 60734-27-2
N-(9H-fluoren-9-ylidene)methanamine

: 38359-28-3
N-methyl-9H-fluoren-9-amine

Guidance literature:: With sodium cyanoborohydride; acetic acid; In methanol; at 40 ℃; for 1h;
DOI:10.1021/ja9624681

Reference yield:

: 486-25-9,952573-42-1
9-fluorenone

: 38359-28-3
N-methyl-9H-fluoren-9-amine

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / TiCl₄ / toluene; CH₂Cl₂ / 2 h / Ambient temperature

2: NaBH₃CN, AcOH / methanol / 1 h / 40 °C

With titanium tetrachloride; sodium cyanoborohydride; acetic acid; In methanol; dichloromethane; toluene;
DOI:10.1021/ja9624681

Reference yield:

: 525-03-1
9-aminofluorene

: 38359-28-3
N-methyl-9H-fluoren-9-amine

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / diethyl ether / 1 h

2: 2.) KOH / 1.) acetone, 30 min, 2.) 80 deg C, 8 h

With potassium hydroxide; In diethyl ether;
DOI:10.1021/jm980440p