4-Pyrimidinamine, 6-chloro-N,2-dimethyl-5-(2-propenyl)-

Base Information

Chemical Name:4-Pyrimidinamine, 6-chloro-N,2-dimethyl-5-(2-propenyl)-
CAS No.:85826-35-3
Molecular Formula:C₉H₁₂ClN₃
Molecular Weight:197.667
Hs Code.:
DSSTox Substance ID:DTXSID10235104
Wikidata:Q83116956

Synonyms:BRN 5005909;85826-35-3;4-Pyrimidinamine, 6-chloro-N,2-dimethyl-5-(2-propenyl)-;6-Chloro-N,2-dimethyl-5-(2-propenyl)-4-pyrimidinamine;6-chloro-N,2-dimethyl-5-(prop-2-en-1-yl)pyrimidin-4-amine;DTXSID10235104;STK022212;LS-134439

Suppliers and Price of 4-Pyrimidinamine, 6-chloro-N,2-dimethyl-5-(2-propenyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-Pyrimidinamine, 6-chloro-N,2-dimethyl-5-(2-propenyl)-

Chemical Property:

Vapor Pressure:0.000578mmHg at 25°C
Boiling Point:311°Cat760mmHg
Flash Point:141.9°C
Density:1.176g/cm³
XLogP3:3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:197.0719751
Heavy Atom Count:13
Complexity:174

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=NC(=C(C(=N1)Cl)CC=C)NC

Technology Process of 4-Pyrimidinamine, 6-chloro-N,2-dimethyl-5-(2-propenyl)-

There total 3 articles about 4-Pyrimidinamine, 6-chloro-N,2-dimethyl-5-(2-propenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.4%

: 85826-33-1
5-Allyl-2-methyl-4,6-dichloropyrimidine

: 74-89-5
methylamine

: 85826-35-3
(5-Allyl-6-chloro-2-methyl-pyrimidin-4-yl)-methyl-amine

Guidance literature:: In ethanol; for 6h; Heating;
DOI:10.1007/BF00765165

Reference yield:

: 2049-80-1
(2-propenyl)propanedioic acid diethyl ester

: 85826-35-3
(5-Allyl-6-chloro-2-methyl-pyrimidin-4-yl)-methyl-amine

Guidance literature:: Multi-step reaction with 3 steps

1: 72.3 percent / CH₃ONa / methanol / 10 h / Heating

2: 60.6 percent / phosphoryl chloride, dimethylaniline / 7 h

3: 85.4 percent / ethanol / 6 h / Heating

With sodium methylate; 2,3-Dimethylaniline; trichlorophosphate; In methanol; ethanol;
DOI:10.1007/BF00765165

Reference yield:

: 85826-32-0
5-Allyl-2-methyl-4,6-dihydroxypyrimidine

: 85826-35-3
(5-Allyl-6-chloro-2-methyl-pyrimidin-4-yl)-methyl-amine

Guidance literature:: Multi-step reaction with 2 steps

1: 60.6 percent / phosphoryl chloride, dimethylaniline / 7 h

2: 85.4 percent / ethanol / 6 h / Heating

With 2,3-Dimethylaniline; trichlorophosphate; In ethanol;
DOI:10.1007/BF00765165