8-(Benzyloxy)-7,7-dimethyloct-5-enoic acid

Base Information

Chemical Name:8-(Benzyloxy)-7,7-dimethyloct-5-enoic acid
CAS No.:89559-97-7
Molecular Formula:C17H24O3
Molecular Weight:276.376
Hs Code.:
DSSTox Substance ID:DTXSID60709062

Synonyms:89559-97-7;8-(Benzyloxy)-7,7-dimethyloct-5-enoic acid;DTXSID60709062

Suppliers and Price of 8-(Benzyloxy)-7,7-dimethyloct-5-enoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 8-(Benzyloxy)-7,7-dimethyloct-5-enoic acid

Chemical Property:

XLogP3:3.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:9
Exact Mass:276.17254462
Heavy Atom Count:20
Complexity:301

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(COCC1=CC=CC=C1)C=CCCCC(=O)O

Technology Process of 8-(Benzyloxy)-7,7-dimethyloct-5-enoic acid

There total 4 articles about 8-(Benzyloxy)-7,7-dimethyloct-5-enoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 38216-93-2
3-benzyloxypivalic aldehyde

: 17814-85-6
(4-carboxybutyl)triphenylphosphonium bromide

: 89559-97-7
7,7-dimethyl-8-(phenylmethoxy)-5(Z)-octenoic acid

Guidance literature:: With sodium hydride; In dimethyl sulfoxide; Ambient temperature;
DOI:10.1002/jps.2600770211

Reference yield:

: 66582-32-9
3-(benzyloxy)-2,2-dimethylpropan-1-ol

: 89559-97-7
7,7-dimethyl-8-(phenylmethoxy)-5(Z)-octenoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 80.5 percent / pyridinium dichromate / CH₂Cl₂ / 96 h

2: 93 percent / NaH / dimethylsulfoxide / Ambient temperature

With dipyridinium dichromate; sodium hydride; In dichloromethane; dimethyl sulfoxide;
DOI:10.1002/jps.2600770211

Reference yield:

: 126-30-7
2,2-Dimethyl-1,3-propanediol

: 89559-97-7
7,7-dimethyl-8-(phenylmethoxy)-5(Z)-octenoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) NaH / 1.) DMF, room temperature, overnight, 2.) 12 h

2: 80.5 percent / pyridinium dichromate / CH₂Cl₂ / 96 h

3: 93 percent / NaH / dimethylsulfoxide / Ambient temperature

With dipyridinium dichromate; sodium hydride; In dichloromethane; dimethyl sulfoxide;
DOI:10.1002/jps.2600770211