3-Pyridinecarboxamide, N-[4-[(dimethylamino)sulfonyl]phenyl]-

Base Information

Chemical Name:3-Pyridinecarboxamide, N-[4-[(dimethylamino)sulfonyl]phenyl]-
CAS No.:89565-39-9
Molecular Formula:C14H15N3O3S
Molecular Weight:305.357
Hs Code.:
DSSTox Substance ID:DTXSID20354092
Wikidata:Q82132046
ChEMBL ID:CHEMBL1462115

Synonyms:MLS000566794;3-Pyridinecarboxamide, N-[4-[(dimethylamino)sulfonyl]phenyl]-;89565-39-9;N-[4-(dimethylsulfamoyl)phenyl]pyridine-3-carboxamide;CHEMBL1462115;DTXSID20354092;HMS2164D13;HMS3316A06;STL495715;AKOS001080916;SMR000153742;Z29266767

Suppliers and Price of 3-Pyridinecarboxamide, N-[4-[(dimethylamino)sulfonyl]phenyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-Pyridinecarboxamide, N-[4-[(dimethylamino)sulfonyl]phenyl]-

Chemical Property:

XLogP3:1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:4
Exact Mass:305.08341252
Heavy Atom Count:21
Complexity:451

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN(C)S(=O)(=O)C1=CC=C(C=C1)NC(=O)C2=CN=CC=C2

Technology Process of 3-Pyridinecarboxamide, N-[4-[(dimethylamino)sulfonyl]phenyl]-

There total 2 articles about 3-Pyridinecarboxamide, N-[4-[(dimethylamino)sulfonyl]phenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 1015067-20-5
4-[(Pyridine-3-carbonyl)-amino]-benzenesulfonyl chloride

: 124-40-3
dimethyl amine

: 89565-39-9
N-(4-(N,N-dimethylsulfamoyl)phenyl)nicotinamide

Guidance literature:

Reference yield:

: 1752-96-1
N-phenylnicotinamide

: 89565-39-9
N-(4-(N,N-dimethylsulfamoyl)phenyl)nicotinamide

Guidance literature:: Multi-step reaction with 2 steps

1: 57 percent / chlorosulfonic acid / 70 - 80 °C

2: 30 percent

With chlorosulfonic acid;

Reference yield: 28.0%

: 27607-77-8
trimethylsilyl trifluoromethanesulfonate

: 89565-39-9
N-(4-(N,N-dimethylsulfamoyl)phenyl)nicotinamide

: 13035-61-5
1,2,3,5-tetraacetylribose

: C₁₉H₂₄N₃O₇S⁽¹⁺⁾*CF₃O₃S^(1-)

Guidance literature:: trimethylsilyl trifluoromethanesulfonate; N-(4-(N,N-dimethylsulfamoyl)phenyl)nicotinamide; 1,2,3,5-tetraacetylribose; In acetonitrile; at 20 ℃; for 2h;

With thionyl chloride; In methanol; at -5 ℃; for 72h; Cooling with ice;