(6-{[tert-Butyl(dimethyl)silyl]oxy}hexyl)(oxo)diphenyl-lambda~5~-phosphane

Base Information

Chemical Name:(6-{[tert-Butyl(dimethyl)silyl]oxy}hexyl)(oxo)diphenyl-lambda~5~-phosphane
CAS No.:89625-22-9
Molecular Formula:C24H37O2PSi
Molecular Weight:416.616
Hs Code.:
DSSTox Substance ID:DTXSID00526750
Wikidata:Q82395526

Synonyms:89625-22-9;DTXSID00526750;(6-{[tert-Butyl(dimethyl)silyl]oxy}hexyl)(oxo)diphenyl-lambda~5~-phosphane

Suppliers and Price of (6-{[tert-Butyl(dimethyl)silyl]oxy}hexyl)(oxo)diphenyl-lambda~5~-phosphane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (6-{[tert-Butyl(dimethyl)silyl]oxy}hexyl)(oxo)diphenyl-lambda~5~-phosphane

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:11
Exact Mass:416.23004395
Heavy Atom Count:28
Complexity:463

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(C)[Si](C)(C)OCCCCCCP(=O)(C1=CC=CC=C1)C2=CC=CC=C2

Technology Process of (6-{[tert-Butyl(dimethyl)silyl]oxy}hexyl)(oxo)diphenyl-lambda~5~-phosphane

There total 4 articles about (6-{[tert-Butyl(dimethyl)silyl]oxy}hexyl)(oxo)diphenyl-lambda~5~-phosphane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 19100-95-9
diphenyl(6-hydroxy-n-hex-1-yl)phosphine oxide

: 18162-48-6
tert-butyldimethylsilyl chloride

: 89625-22-9
1-(6-tert-Butyldimethylsilyloxyhexyl)diphenylphosphine Oxide

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide;

Reference yield:

: [5-(carboxy)pentyl]triphenylphosphonium

: 89625-22-9
1-(6-tert-Butyldimethylsilyloxyhexyl)diphenylphosphine Oxide

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / 30percent aq. NaOH / 0.5 h / Heating

2: 96 percent / conc. H₂SO₄, 4 Angstroem molecular sieves / Heating

3: 94 percent / LiBH₄ / tetrahydrofuran

4: 92 percent / imidazole / dimethylformamide

With 1H-imidazole; sodium hydroxide; lithium borohydride; 4 A molecular sieve; sulfuric acid; In tetrahydrofuran; N,N-dimethyl-formamide;

Reference yield:

: 73367-77-8
(5-carboxypentyl)diphenylphosphine oxide

: 89625-22-9
1-(6-tert-Butyldimethylsilyloxyhexyl)diphenylphosphine Oxide

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / conc. H₂SO₄, 4 Angstroem molecular sieves / Heating

2: 94 percent / LiBH₄ / tetrahydrofuran

3: 92 percent / imidazole / dimethylformamide

With 1H-imidazole; lithium borohydride; 4 A molecular sieve; sulfuric acid; In tetrahydrofuran; N,N-dimethyl-formamide;