2-(2-Hydroxybenzoyl)-3-nitrobenzoic acid

Base Information

Chemical Name:2-(2-Hydroxybenzoyl)-3-nitrobenzoic acid
CAS No.:89646-23-1
Molecular Formula:C14H9NO6
Molecular Weight:287.229
Hs Code.:
DSSTox Substance ID:DTXSID10522061
Wikidata:Q82387000

Synonyms:2-(2-Hydroxybenzoyl)-3-nitrobenzoic acid;89646-23-1;DTXSID10522061

Suppliers and Price of 2-(2-Hydroxybenzoyl)-3-nitrobenzoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 2-(2-Hydroxybenzoyl)-3-nitrobenzoic acid

Chemical Property:

XLogP3:2.8
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:3
Exact Mass:287.04298701
Heavy Atom Count:21
Complexity:432

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C(=C1)C(=O)C2=C(C=CC=C2[N+](=O)[O-])C(=O)O)O

Technology Process of 2-(2-Hydroxybenzoyl)-3-nitrobenzoic acid

There total 1 articles about 2-(2-Hydroxybenzoyl)-3-nitrobenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.5%

: 641-70-3
3-nitrophthalic acid anhydride

: 108-95-2,27073-41-2
phenol

: 89646-23-1
2-(2-Hydroxybenzoyl)-3-nitro-benzoesaeure

Guidance literature:: With aluminium trichloride; at 110 - 120 ℃; for 3h;
DOI:10.1002/ardp.19843170206

Reference yield: 83.3%

: 89646-23-1
2-(2-Hydroxybenzoyl)-3-nitro-benzoesaeure

: 89646-24-2
3-Amino-2-(2-hydroxybenzoyl)-benzoesaeure

Guidance literature:: With hydrogen; nickel; In ethanol; Ambient temperature;
DOI:10.1002/ardp.19843170206

Reference yield:

: 89646-23-1
2-(2-Hydroxybenzoyl)-3-nitro-benzoesaeure

: 1143-38-0
1,8-dihydroxy-9(10H)-anthracenone

Guidance literature:: Multi-step reaction with 4 steps

1: 83.3 percent / H₂ / Raney-Nickel / ethanol / Ambient temperature

2: 81.7 percent / 17percent aq. HCl, NaNO₂

3: 38.4 percent / conc. H₂SO₄, H₂SO₄(65percent SO₃), boric acid / 0.5 h / 120 °C

4: 93.7 percent

With hydrogenchloride; sulfuric acid; sulfur trioxide; hydrogen; boric acid; sodium nitrite; nickel; In ethanol;
DOI:10.1002/ardp.19843170206