3-Hydroxy-2-(2-hydroxybenzoyl)benzoic acid

Base Information

Chemical Name:3-Hydroxy-2-(2-hydroxybenzoyl)benzoic acid
CAS No.:89646-25-3
Molecular Formula:C14H10O5
Molecular Weight:258.23
Hs Code.:
DSSTox Substance ID:DTXSID30522063
Wikidata:Q82387003

Synonyms:89646-25-3;3-Hydroxy-2-(2-hydroxybenzoyl)benzoic acid;DTXSID30522063

Suppliers and Price of 3-Hydroxy-2-(2-hydroxybenzoyl)benzoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-Hydroxy-2-(2-hydroxybenzoyl)benzoic acid

Chemical Property:

XLogP3:2.6
Hydrogen Bond Donor Count:3
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:3
Exact Mass:258.05282342
Heavy Atom Count:19
Complexity:354

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C(=C1)C(=O)C2=C(C=CC=C2O)C(=O)O)O

Technology Process of 3-Hydroxy-2-(2-hydroxybenzoyl)benzoic acid

There total 4 articles about 3-Hydroxy-2-(2-hydroxybenzoyl)benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.7%

: 89646-24-2
3-Amino-2-(2-hydroxybenzoyl)-benzoesaeure

: 89646-25-3
3-Hydroxy-2-(2-hydroxybenzoyl)-benzoesaeure

Guidance literature:: With hydrogenchloride; sodium nitrite;
DOI:10.1002/ardp.19843170206

Reference yield:

: 89646-23-1
2-(2-Hydroxybenzoyl)-3-nitro-benzoesaeure

: 89646-25-3
3-Hydroxy-2-(2-hydroxybenzoyl)-benzoesaeure

Guidance literature:: Multi-step reaction with 2 steps

1: 83.3 percent / H₂ / Raney-Nickel / ethanol / Ambient temperature

2: 81.7 percent / 17percent aq. HCl, NaNO₂

With hydrogenchloride; hydrogen; sodium nitrite; nickel; In ethanol;
DOI:10.1002/ardp.19843170206

Reference yield:

: 641-70-3
3-nitrophthalic acid anhydride

: 89646-25-3
3-Hydroxy-2-(2-hydroxybenzoyl)-benzoesaeure

Guidance literature:: Multi-step reaction with 3 steps

1: aluminium chloride / 135 °C

2: iron (II)-hydroxide; aqueous ammonia

3: ueber die Diazonium-Verbindung

With ammonium hydroxide; aluminium trichloride; iron(II) hydroxide;