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3,7-diphenyl-5,6-dihydro-4H-1,2-diazepine

Base Information Edit
  • Chemical Name:3,7-diphenyl-5,6-dihydro-4H-1,2-diazepine
  • CAS No.:13338-06-2
  • Molecular Formula:C17H16 N2
  • Molecular Weight:248.3223
  • Hs Code.:
  • Mol file:13338-06-2.mol
3,7-diphenyl-5,6-dihydro-4H-1,2-diazepine

Synonyms:NSC148978; NSC 620115

Suppliers and Price of 3,7-diphenyl-5,6-dihydro-4H-1,2-diazepine
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The product has achieved commercial mass production*data from LookChem market partment
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Total 3 raw suppliers
Chemical Property of 3,7-diphenyl-5,6-dihydro-4H-1,2-diazepine Edit
Chemical Property:
  • Vapor Pressure:3.35E-05mmHg at 25°C 
  • Boiling Point:365.2°Cat760mmHg 
  • Flash Point:167°C 
  • Density:1.07g/cm3 
Purity/Quality:
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MSDS Files:

SDS file from LookChem

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Technology Process of 3,7-diphenyl-5,6-dihydro-4H-1,2-diazepine

There total 7 articles about 3,7-diphenyl-5,6-dihydro-4H-1,2-diazepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
5-(tert-butylperoxy)-1,5-diphenylpentan-1-one; With 1,8-diazabicyclo[5.4.0]undec-7-ene; In acetonitrile; at 50 ℃; for 1h; Schlenk technique;
With hydrazine hydrate; In ethanol; at 80 ℃; for 12h; Schlenk technique;
DOI:10.1021/acs.orglett.1c02824
Guidance literature:
With hydrogenchloride; hydrazine hydrate;
DOI:10.1021/ja01598a075
Guidance literature:
Multi-step reaction with 2 steps
1.1: iron(III)-acetylacetonate / 1,2-dichloro-ethane / 8 h / 70 °C / Inert atmosphere; Schlenk technique
2.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 1 h / 50 °C / Schlenk technique
2.2: 12 h / 80 °C / Schlenk technique
With iron(III)-acetylacetonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; In 1,2-dichloro-ethane; acetonitrile;
DOI:10.1021/acs.orglett.1c02824
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