Silane, trimethyl[(1-phenylcyclopropyl)oxy]-

Base Information

Chemical Name:Silane, trimethyl[(1-phenylcyclopropyl)oxy]-
CAS No.:38858-73-0
Molecular Formula:C12H18OSi
Molecular Weight:206.36
Hs Code.:
DSSTox Substance ID:DTXSID30474093
Nikkaji Number:J403.165B
Wikidata:Q82303878
Mol file:38858-73-0.mol

Synonyms:38858-73-0;Silane, trimethyl[(1-phenylcyclopropyl)oxy]-;DTXSID30474093

Suppliers and Price of Silane, trimethyl[(1-phenylcyclopropyl)oxy]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Silane, trimethyl[(1-phenylcyclopropyl)oxy]-

Chemical Property:

Boiling Point:90-95 °C(Press: 10 Torr)
PSA：9.23000
Density:0.97±0.1 g/cm3(Predicted)
LogP:3.52720
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:206.112691728
Heavy Atom Count:14
Complexity:197

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C[Si](C)(C)OC1(CC1)C2=CC=CC=C2

Technology Process of Silane, trimethyl[(1-phenylcyclopropyl)oxy]-

There total 8 articles about Silane, trimethyl[(1-phenylcyclopropyl)oxy]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 75-77-4
chloro-trimethyl-silane

: 7257-94-5
1-phenyl-2-(p-tolylsulfonyloxy)ethanone

: 31729-70-1
bis(iodozinc)methane

: 38858-73-0
1-phenyl-1-trimethylsiloxycyclopropane

Guidance literature:: 1-phenyl-2-(p-tolylsulfonyloxy)ethanone; bis(iodozinc)methane; In tetrahydrofuran; at 25 ℃; for 2h;

chloro-trimethyl-silane; In tetrahydrofuran; for 0.5h;
DOI:10.1002/asia.200900289

Reference yield: 86.0%

: 13735-81-4
1-styrenyloxytrimethylsilane

: 75-11-6
diiodomethane

: 38858-73-0
1-phenyl-1-trimethylsiloxycyclopropane

Guidance literature:: With triethylaluminum; In hexane; Ambient temperature;
DOI:10.1021/jo00222a051

Reference yield:

: 98-86-2
acetophenone

: 38858-73-0
1-phenyl-1-trimethylsiloxycyclopropane

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 0 °C / Inert atmosphere

2: diethylzinc / dichloromethane; tetrahydrofuran / 16 h / 0 - 20 °C / Inert atmosphere

With diethylzinc; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1039/c5ob00632e