Technology Process of Pyridine, 2-(1-phenylethyl)-, (R)-
There total 10 articles about Pyridine, 2-(1-phenylethyl)-, (R)- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tri-n-butyl-tin hydride;
In
toluene;
for 0.333333h;
Reflux;
DOI:10.1002/anie.201602264
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1,2-dichloro-ethane; triethylamine / dichloromethane / 2 h / 0 - 20 °C
2: tetrahydrofuran / 4 h / 0 - 20 °C
3: potassium tert-butylate / tetrahydrofuran / 1 h / 0 - 20 °C
4: nicotinamide adenine dinucleotide phosphate; tris(2,2'-bipyridyl)ruthenium dichloride; D-glucose; glucose dehydrogenase-105; ene reductase from N. punctiforme / isopropyl alcohol / 48 h / 4 °C / pH 9 / Irradiation; Enzymatic reaction
With
tris(2,2'-bipyridyl)ruthenium dichloride; D-glucose; glucose dehydrogenase-105; potassium tert-butylate; ene reductase from N. punctiforme; nicotinamide adenine dinucleotide phosphate; 1,2-dichloro-ethane; triethylamine;
In
tetrahydrofuran; dichloromethane; isopropyl alcohol;
DOI:10.1002/anie.202003125