1-Methyl-4-({[(4-nitrophenyl)methyl]sulfanyl}methyl)benzene

Base Information

Chemical Name:1-Methyl-4-({[(4-nitrophenyl)methyl]sulfanyl}methyl)benzene
CAS No.:89845-91-0
Molecular Formula:C₁₅H₁₅NO₂S
Molecular Weight:273.356
Hs Code.:
DSSTox Substance ID:DTXSID00531642
Wikidata:Q82403650

Synonyms:89845-91-0;DTXSID00531642;1-Methyl-4-({[(4-nitrophenyl)methyl]sulfanyl}methyl)benzene

Suppliers and Price of 1-Methyl-4-({[(4-nitrophenyl)methyl]sulfanyl}methyl)benzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 1-Methyl-4-({[(4-nitrophenyl)methyl]sulfanyl}methyl)benzene

Chemical Property:

XLogP3:4.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:273.08234989
Heavy Atom Count:19
Complexity:276

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)CSCC2=CC=C(C=C2)[N+](=O)[O-]

Technology Process of 1-Methyl-4-({[(4-nitrophenyl)methyl]sulfanyl}methyl)benzene

There total 2 articles about 1-Methyl-4-({[(4-nitrophenyl)methyl]sulfanyl}methyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 104-82-5
4-Methylbenzyl chloride

: 89845-91-0
4-methyl-4'-nitrodibenzyl sulphide

Guidance literature:: Multi-step reaction with 2 steps

1: CHCl₃ / 1 h / Heating

2: TBAB / benzene; aq. NaOH / 1.5 h / Ambient temperature

tetrabutylammomium bromide; In sodium hydroxide; chloroform; benzene;
DOI:10.1055/s-1987-28085

Reference yield:

: 100-14-1
4-nitrobenzyl chloride

: 58174-34-8
S-(4-methylbenzyl) thioacetimidate hydrochloride

: 89845-91-0
4-methyl-4'-nitrodibenzyl sulphide

Guidance literature:: tetrabutylammomium bromide; In sodium hydroxide; benzene; for 1.5h; Yield given; Ambient temperature;
DOI:10.1055/s-1987-28085

Reference yield: 68.0%

: 3375-31-3
palladium diacetate

: 89845-91-0
4-methyl-4'-nitrodibenzyl sulphide

: (Pd(C₆H₃(CH₃)CH₂SCH₂C₆H₄NO₂)(O₂CCH₃))2

Guidance literature:: In acetic acid; suspn. of Pd(CH3CO2)2 and ligand (molar ratio 1:1.1) in acetic acid washeated at 70°C for 8 h; filtered, recrystd. from CH2Cl2 and hexane; elem. anal.;