Technology Process of Ethanone, 1-(6-phenyl-4-pyrimidinyl)-, oxime
There total 4 articles about Ethanone, 1-(6-phenyl-4-pyrimidinyl)-, oxime which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogenchloride; n-propyl nitrite;
In
ethanol;
for 2h;
Ambient temperature;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 96 percent / hydrogen/conc. ammonia / 5percent palladium charcoal / methanol
2: 79 percent / propyl nitrite, HCl / ethanol / 2 h / Ambient temperature
With
hydrogenchloride; ammonium hydroxide; n-propyl nitrite; hydrogen;
palladium on activated charcoal;
In
methanol; ethanol;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 85 percent / phosphoryl chloride / 3 h / Heating
2: 96 percent / hydrogen/conc. ammonia / 5percent palladium charcoal / methanol
3: 79 percent / propyl nitrite, HCl / ethanol / 2 h / Ambient temperature
With
hydrogenchloride; ammonium hydroxide; n-propyl nitrite; hydrogen; trichlorophosphate;
palladium on activated charcoal;
In
methanol; ethanol;
