5-(Bromomethyl)-4,4-dimethyl-2-phenyl-1,3-dioxolane

Base Information

Chemical Name:5-(Bromomethyl)-4,4-dimethyl-2-phenyl-1,3-dioxolane
CAS No.:89995-41-5
Molecular Formula:C₁₂H₁₅BrO₂
Molecular Weight:271.154
Hs Code.:
DSSTox Substance ID:DTXSID30527593

Synonyms:89995-41-5;5-(Bromomethyl)-4,4-dimethyl-2-phenyl-1,3-dioxolane;DTXSID30527593

Suppliers and Price of 5-(Bromomethyl)-4,4-dimethyl-2-phenyl-1,3-dioxolane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 5-(Bromomethyl)-4,4-dimethyl-2-phenyl-1,3-dioxolane

Chemical Property:

XLogP3:2.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:270.02554
Heavy Atom Count:15
Complexity:212

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1(C(OC(O1)C2=CC=CC=C2)CBr)C

Technology Process of 5-(Bromomethyl)-4,4-dimethyl-2-phenyl-1,3-dioxolane

There total 1 articles about 5-(Bromomethyl)-4,4-dimethyl-2-phenyl-1,3-dioxolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 1120-79-2
1-bromomethyl-2,2-dimethyloxirane

: 100-52-7
benzaldehyde

: 89995-41-5
5-Bromomethyl-4,4-dimethyl-2-phenyl-[1,3]dioxolane

Guidance literature:: With boron trifluoride diethyl etherate; Heating;
DOI:10.1007/BF00842826

Reference yield: 59.0%

: 89995-41-5
5-Bromomethyl-4,4-dimethyl-2-phenyl-[1,3]dioxolane

: 22940-38-1
4,4-dimethyl-5-methylene-2-phenyl-1,3-dioxolane

Guidance literature:: With diethylene glycol monosodium salt; at 60 - 70 ℃; for 3h;
DOI:10.1007/BF00842826

Reference yield:

: 89995-41-5
5-Bromomethyl-4,4-dimethyl-2-phenyl-[1,3]dioxolane

: 89995-61-9
5-[1,2-Dichloro-eth-(Z)-ylidene]-4,4-dimethyl-2-phenyl-[1,3]dioxolane

Guidance literature:: Multi-step reaction with 3 steps

1: 59 percent / natrium diethylene glycolate / 3 h / 60 - 70 °C

2: 75 percent / 50percent aq. NaOH, TEBA / Ambient temperature

3: 70 percent / benzene / 1 h / Heating

With sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; diethylene glycol monosodium salt; In benzene;
DOI:10.1007/BF00842826