Technology Process of Heptanoic acid, 3-ethyl-,
1-[[[bis(phenylmethoxy)phosphinyl]oxy]methyl]-1,2-ethanediyl ester
There total 4 articles about Heptanoic acid, 3-ethyl-,
1-[[[bis(phenylmethoxy)phosphinyl]oxy]methyl]-1,2-ethanediyl ester which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dmap; dicyclohexyl-carbodiimide;
In
dichloromethane;
at 0 - 20 ℃;
DOI:10.1002/chem.200501422
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 55 percent / Dowex 5W-X8(H+) resin / methanol / 48 h
2: 63 percent / dicyclohexylcarbodiimide; dimethylaminopyridine / CH2Cl2 / 0 - 20 °C
With
dmap; Dowex 5W-X8(H+) resin; dicyclohexyl-carbodiimide;
In
methanol; dichloromethane;
DOI:10.1002/chem.200501422
- Guidance literature:
-
Multi-step reaction with 4 steps
1: chlorosuccinimide / toluene / 2 h / 20 °C
2: 29 percent / pyridine / 2 h / 0 °C
3: 55 percent / Dowex 5W-X8(H+) resin / methanol / 48 h
4: 63 percent / dicyclohexylcarbodiimide; dimethylaminopyridine / CH2Cl2 / 0 - 20 °C
With
dmap; N-chloro-succinimide; Dowex 5W-X8(H+) resin; dicyclohexyl-carbodiimide;
In
pyridine; methanol; dichloromethane; toluene;
DOI:10.1002/chem.200501422
