1-Benzyl-5-(benzyloxy)pyridin-2(1H)-one

Base Information

Chemical Name:1-Benzyl-5-(benzyloxy)pyridin-2(1H)-one
CAS No.:90292-53-8
Molecular Formula:C19H17NO2
Molecular Weight:291.349
Hs Code.:
DSSTox Substance ID:DTXSID60560150
Wikidata:Q82443148

Synonyms:1-Benzyl-5-(benzyloxy)pyridin-2(1H)-one;90292-53-8;DTXSID60560150

Suppliers and Price of 1-Benzyl-5-(benzyloxy)pyridin-2(1H)-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-Benzyl-5-(benzyloxy)pyridin-2(1H)-one

Chemical Property:

XLogP3:3.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:5
Exact Mass:291.125928785
Heavy Atom Count:22
Complexity:429

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)CN2C=C(C=CC2=O)OCC3=CC=CC=C3

Technology Process of 1-Benzyl-5-(benzyloxy)pyridin-2(1H)-one

There total 7 articles about 1-Benzyl-5-(benzyloxy)pyridin-2(1H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 5154-01-8,24154-26-5
2,5-dihydroxypyridine

: 100-44-7
benzyl chloride

: 90292-53-8
5-benzyloxy-N-benzylpyridine-2-one

Guidance literature:: With potassium hydroxide; In dimethyl sulfoxide; for 1h;
DOI:10.1002/ardp.19843170405

Reference yield:

: 142-08-5,1199357-22-6
2-Pyridone

: 90292-53-8
5-benzyloxy-N-benzylpyridine-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: 34 percent / Elbs oxidation

2: 54 percent / KOH / dimethylsulfoxide / 1 h

With potassium hydroxide; In dimethyl sulfoxide;
DOI:10.1002/ardp.19843170405

Reference yield:

: 100-39-0
benzyl bromide

: 90292-53-8
5-benzyloxy-N-benzylpyridine-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / 66 h / Reflux; Inert atmosphere

2: sodium tetrahydroborate / Inert atmosphere

With sodium tetrahydroborate; In toluene;
DOI:10.3987/COM-11-12239