Propanamide, 3-[[3-(3,5-dichlorophenyl)-1-(2-naphthalenyl)-1H-pyrazol-5-yl]oxy]-N-[4-[[ (1,1-dimethylethyl)diphenylsilyl]oxy]-1-(1-methylethyl)butyl]-

Base Information

Chemical Name:Propanamide, 3-[[3-(3,5-dichlorophenyl)-1-(2-naphthalenyl)-1H-pyrazol-5-yl]oxy]-N-[4-[[ (1,1-dimethylethyl)diphenylsilyl]oxy]-1-(1-methylethyl)butyl]-
CAS No.:907190-80-1
Molecular Formula:C45H49Cl2N3O3Si
Molecular Weight:778.894
Hs Code.:

Propanamide,
3-[[3-(3,5-dichlorophenyl)-1-(2-naphthalenyl)-1H-pyrazol-5-yl]oxy]-N-[4-[[
(1,1-dimethylethyl)diphenylsilyl]oxy]-1-(1-methylethyl)butyl]-

Synonyms:

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Chemical Property of Propanamide, 3-[[3-(3,5-dichlorophenyl)-1-(2-naphthalenyl)-1H-pyrazol-5-yl]oxy]-N-[4-[[ (1,1-dimethylethyl)diphenylsilyl]oxy]-1-(1-methylethyl)butyl]-

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Technology Process of Propanamide, 3-[[3-(3,5-dichlorophenyl)-1-(2-naphthalenyl)-1H-pyrazol-5-yl]oxy]-N-[4-[[ (1,1-dimethylethyl)diphenylsilyl]oxy]-1-(1-methylethyl)butyl]-

There total 11 articles about Propanamide, 3-[[3-(3,5-dichlorophenyl)-1-(2-naphthalenyl)-1H-pyrazol-5-yl]oxy]-N-[4-[[ (1,1-dimethylethyl)diphenylsilyl]oxy]-1-(1-methylethyl)butyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 907190-76-5
4-{[tert-butyl(diphenyl)silyl]oxy}-1-(isopropylbutyl)amine

: 907190-79-8
3-{[3-(3,5-dichlorophenyl)-1-(2-naphthyl)-1H-pyrazol-5-yl]oxy}propanoic acid

: 907190-80-1
N-(4-{[tert-butyl(diphenyl)silyl]oxy}-1-isopropylbutyl)-3-{[3-(3,5-dichlorophenyl)-1-(2-naphthyl)-1H-pyrazol-5-yl]oxy}propanamide

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 40 ℃;
DOI:10.1016/j.bmcl.2006.10.060

Reference yield:

: 907190-73-2
6-{[tert-butyl(diphenyl)silyl]oxy}-2-methylhexan-3-ol

: 907190-80-1
N-(4-{[tert-butyl(diphenyl)silyl]oxy}-1-isopropylbutyl)-3-{[3-(3,5-dichlorophenyl)-1-(2-naphthyl)-1H-pyrazol-5-yl]oxy}propanamide

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / 0 °C

2: NaN₃ / dimethylformamide / 40 °C

3: H₂ / Pd/C / methanol; ethyl acetate / 20 °C

4: 65 percent / EDCI; DMAP / dimethylformamide / 40 °C

With pyridine; dmap; sodium azide; hydrogen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; palladium on activated charcoal; In methanol; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2006.10.060

Reference yield:

: 907190-75-4
[(4-azido-5-methylhexyl)oxy](tert-butyl)diphenylsilane

: 907190-80-1
N-(4-{[tert-butyl(diphenyl)silyl]oxy}-1-isopropylbutyl)-3-{[3-(3,5-dichlorophenyl)-1-(2-naphthyl)-1H-pyrazol-5-yl]oxy}propanamide

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / Pd/C / methanol; ethyl acetate / 20 °C

2: 65 percent / EDCI; DMAP / dimethylformamide / 40 °C

With dmap; hydrogen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; palladium on activated charcoal; In methanol; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2006.10.060