Benzenepropanoyl chloride, 2-bromo-

Base Information

Chemical Name:Benzenepropanoyl chloride, 2-bromo-
CAS No.:90725-40-9
Molecular Formula:C9H8BrClO
Molecular Weight:247.519
Hs Code.:2916399090
Mol file:90725-40-9.mol

Synonyms:3-(2-Bromophenyl)propionic acid chloride;3-(2-Bromophenyl)propionyl chloride;Hydrocinnamoyl chloride, o-bromo-;

Suppliers and Price of Benzenepropanoyl chloride, 2-bromo-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of Benzenepropanoyl chloride, 2-bromo-

Chemical Property:

PSA：17.07000
LogP:3.14710

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzenepropanoyl chloride, 2-bromo-

There total 8 articles about Benzenepropanoyl chloride, 2-bromo- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 15115-58-9
3-(2-bromophenyl)propionic acid

: 90725-40-9
3-(2-bromophenyl)propanoyl chloride

Guidance literature:: With oxalyl dichloride; In dichloromethane; N,N-dimethyl-formamide; at 20 ℃; for 1h;
DOI:10.1016/j.bmc.2017.07.028

Reference yield:

: 3433-80-5
1-Bromo-2-bromomethyl-benzene

: 90725-40-9
3-(2-bromophenyl)propanoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: NaOEt / ethanol / 19 h / Heating

1.2: aq. NaOH / 3 h / Heating

1.3: 51 percent / aq. HCl / 12 h / Heating

2.1: SOCl₂; DMF / CH₂Cl₂ / 22 h / Heating

With thionyl chloride; sodium ethanolate; N,N-dimethyl-formamide; In ethanol; dichloromethane;
DOI:10.1021/ja028301r