Benzoic acid, 4-[(1E)-3-ethoxy-3-oxo-1-propenyl]-

Base Information

Chemical Name:Benzoic acid, 4-[(1E)-3-ethoxy-3-oxo-1-propenyl]-
CAS No.:91047-75-5
Molecular Formula:C12H12O4
Molecular Weight:220.225
Hs Code.:
Mol file:91047-75-5.mol

Synonyms:(E)-4-(3-ethoxy-3-oxoprop-1-enyl)benzoic acid;ethyl 4-carboxycinnamate;(E)-ethyl 4-hydroxycarbonylcinnamate;4-carboxycinnamic acid ethyl ester;(E)-4-(3-ethoxy-3-oxoprop-1-en-1-yl)benzoic acid;4-((E)-2-(ethoxycarbonyl)vinyl)benzoic acid;4-((E)-2-Ethoxycarbonyl-vinyl)-benzoic acid;

Suppliers and Price of Benzoic acid, 4-[(1E)-3-ethoxy-3-oxo-1-propenyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
(E)-4-(3-ETHOXY-3-OXOPROP-1-EN-1-YL)BENZOIC ACID 95.00%
5MG
$ 499.00

Total 2 raw suppliers

Chemical Property of Benzoic acid, 4-[(1E)-3-ethoxy-3-oxo-1-propenyl]-

Chemical Property:

Melting Point:191 - 194 °C
PSA：63.60000
LogP:1.96110

Purity/Quality:: (E)-4-(3-ETHOXY-3-OXOPROP-1-EN-1-YL)BENZOIC ACID 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of Benzoic acid, 4-[(1E)-3-ethoxy-3-oxo-1-propenyl]-

There total 9 articles about Benzoic acid, 4-[(1E)-3-ethoxy-3-oxo-1-propenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 619-66-9
4-Carboxybenzaldehyde

: 105-36-2
ethyl bromoacetate

: 91047-75-5
ethyl (E)-3-[4-(hydroxycarbonyl)phenyl]prop-2-enoate

Guidance literature:: With triphenylphosphine; nanocrystalline aerogel prepared MgO; In N,N-dimethyl-formamide; at 20 ℃; for 7h;
DOI:10.1002/adsc.200606001

Reference yield: 84.0%

: 619-66-9
4-Carboxybenzaldehyde

: 1099-45-2
ethyl (triphenylphosphoranylidene)acetate

: 91047-75-5
ethyl (E)-3-[4-(hydroxycarbonyl)phenyl]prop-2-enoate

Guidance literature:: In dichloromethane; for 4h; Reflux;
DOI:10.1016/j.bmcl.2017.09.056

Reference yield: 81.0%

: 619-58-9
4-iodobenzoic acid

: 140-88-5,9003-32-1
ethyl acrylate

: 91047-75-5
ethyl (E)-3-[4-(hydroxycarbonyl)phenyl]prop-2-enoate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 110 ℃; for 6h; Inert atmosphere;
DOI:10.1016/j.tetlet.2012.10.062