(E)-3-(4-(hydrazinecarbonyl)phenyl)-N-hydroxyacrylaMide hydrochloride

Base Information

Chemical Name:(E)-3-(4-(hydrazinecarbonyl)phenyl)-N-hydroxyacrylaMide hydrochloride
CAS No.:1223593-75-6
Molecular Formula:C₁₀H₁₁N₃O₃*ClH
Molecular Weight:257.677
Hs Code.:
Mol file:1223593-75-6.mol

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-3-(4-(hydrazinecarbonyl)phenyl)-N-hydroxyacrylaMide hydrochloride

Chemical Property:

Purity/Quality:

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Technology Process of (E)-3-(4-(hydrazinecarbonyl)phenyl)-N-hydroxyacrylaMide hydrochloride

There total 10 articles about (E)-3-(4-(hydrazinecarbonyl)phenyl)-N-hydroxyacrylaMide hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.9%

: 1223593-73-4
(E)-tert-butyl 2-(4-(3-(hydroxyamino)-3-oxoprop-1-enyl)benzoyl)hydrazinecarboxylate

: 1223593-75-6
(E)-3-(4-(hydrazinecarbonyl)phenyl)-N-hydroxyacrylamide hydrochloride

Guidance literature:: With hydrogenchloride; In methanol; at 20 ℃; for 1h;

Reference yield: 84.9%

: 1538582-58-9
C₁₅H₁₉N₃O₅

: 1538582-59-0,1223593-75-6
C₁₀H₁₁N₃O₃*ClH

Guidance literature:: With hydrogenchloride; In methanol; at 20 ℃; for 1h;

Reference yield:

: 619-66-9
4-Carboxybenzaldehyde

: 1223593-75-6
(E)-3-(4-(hydrazinecarbonyl)phenyl)-N-hydroxyacrylamide hydrochloride

Guidance literature:: Multi-step reaction with 5 steps

1.1: piperidine / pyridine / 18 h / 100 °C / Inert atmosphere

1.2: 0 °C

2.1: triethylamine; methyl chloroformate / dichloromethane / 1 h / 0 °C

3.1: dmap / dichloromethane / 3 h / 20 °C

4.1: hydroxylamine hydrochloride; sodium hydroxide / ethanol; methanol / 18 h

5.1: hydrogenchloride / methanol / 1 h / 20 °C

With piperidine; hydrogenchloride; hydroxylamine hydrochloride; triethylamine; methyl chloroformate; sodium hydroxide; dmap; In pyridine; methanol; ethanol; dichloromethane;