Benzene, (5-methoxy-1,3-pentadiynyl)-

Base Information

Chemical Name:Benzene, (5-methoxy-1,3-pentadiynyl)-
CAS No.:91368-24-0
Molecular Formula:C12H10O
Molecular Weight:170.211
Hs Code.:
DSSTox Substance ID:DTXSID70449563
Nikkaji Number:J533.550G

Synonyms:91368-24-0;Benzene, (5-methoxy-1,3-pentadiynyl)-;DTXSID70449563;1-Phenyl-5-methoxy-1,3-pentadiyne;(5-methoxy-penta-1,3-diynyl)-benzene

Suppliers and Price of Benzene, (5-methoxy-1,3-pentadiynyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzene, (5-methoxy-1,3-pentadiynyl)-

Chemical Property:

XLogP3:2.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:170.073164938
Heavy Atom Count:13
Complexity:259

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COCC#CC#CC1=CC=CC=C1

Technology Process of Benzene, (5-methoxy-1,3-pentadiynyl)-

There total 4 articles about Benzene, (5-methoxy-1,3-pentadiynyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 536-74-3
phenylacetylene

: 627-41-8
propargyl alcohol methyl ether

: 91368-24-0
(5-methoxy penta-1,3-diyn-1-yl)benzene

Guidance literature:: With copper(l) iodide; nickel(II) chloride hexahydrate; N,N,N,N,-tetramethylethylenediamine; oxygen; In tetrahydrofuran; at 20 ℃; for 20h;
DOI:10.1021/ol8027863

Reference yield: 88.0%

: 932-87-6
1-Bromo-2-phenylacetylene

: 627-41-8
propargyl alcohol methyl ether

: 91368-24-0
(5-methoxy penta-1,3-diyn-1-yl)benzene

Guidance literature:: propargyl alcohol methyl ether; With copper(l) iodide; P-olefin; triethylamine; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In N,N-dimethyl-formamide; for 0.0833333h; Inert atmosphere;

1-Bromo-2-phenylacetylene; In N,N-dimethyl-formamide; at 20 ℃; for 9h; Inert atmosphere;
DOI:10.1021/ja8049436

Reference yield: 81.0%

: 1-(phenylethynyl)-3,3-bis(trifluoromethyl)-1,3-dihydro-1λ³-benzo[d][1,2]iodaoxole

: 627-41-8
propargyl alcohol methyl ether

: 91368-24-0
(5-methoxy penta-1,3-diyn-1-yl)benzene

Guidance literature:: With 1,10-Phenanthroline; triazole; silver(I) 4-methylbenzenesulfonate; In acetonitrile; at 20 ℃; for 4h; Schlenk technique; Inert atmosphere;
DOI:10.1002/anie.201702833